Carbonate Mudstone Chemofacies Zonation Using HH-XRF and PCA

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Solution Overview

Problem

Traditional methods for stratigraphic zonation and correlation of basinal carbonate mudstones face challenges due to their fine-grained and heterogeneous nature, leading to suboptimal resolution of lithofacies changes and requiring extensive expert interpretation, which are time-consuming and costly.

Innovation Solution

A method and system utilizing handheld X-ray fluorescence (HH-XRF) for high-vertical resolution analysis, combined with Principal Component Analysis (PCA) and Hierarchical Clustering on Principal Components (HCPC), to generate chemofacies and delineate stratigraphic zones, enabling efficient and non-destructive characterization of mudstone cores.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If traditional methods (wireline well logs and seismic data) are used for stratigraphic zonation, then the process is simpler and faster, but the resolution of lithofacies changes is insufficient due to the fine-grained nature of mudstones

Engineering Contradiction:
Improveresolution of lithofacies changesVSAvoidcomplexity of analysis method
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent replaces traditional mechanical/measurement-based methods (wireline well logs, seismic data) with chemical analysis methods (handheld XRF spectroscopy). This substitution enables detection of fine-grained lithofacies changes through chemical composition analysis, achieving superior resolution without requiring complex mechanical measurement systems.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the measurement parameter from physical properties (acoustic, seismic, electrical) to chemical composition parameters. By analyzing elemental concentrations via XRF spectroscopy, the method captures subtle compositional variations in mudstones that traditional physical measurement methods cannot resolve, thereby improving lithofacies detection precision.

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If chemostratigraphic data from inorganic geochemical analyses is used, then the detail of compositional variability is improved, but the time and expertise required for interpretation increases

Engineering Contradiction:
Improvedetail of compositional variabilityVSAvoidtime for expert interpretation
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent applies automated multivariate statistical analysis (PCA, HCPC, k-means clustering) that processes geochemical data independently without requiring extensive expert intervention. The system automatically identifies chemofacies, delineates stratigraphic zones, and performs well-to-well correlation, reducing the time and expertise needed compared to traditional manual interpretation methods.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent replaces manual expert interpretation with automated computational analysis. Multivariate statistical algorithms automatically process geochemical datasets, identify patterns, and generate stratigraphic frameworks, substituting human expertise with automated systems that achieve comparable or superior analysis speed and consistency.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Measurement precision

If handheld XRF analysis is performed at high-vertical resolution intervals, then the accuracy of stratigraphic zonation is improved, but the number of measurements and data processing complexity increases

Engineering Contradiction:
Improveaccuracy of stratigraphic zonationVSAvoidcomplexity of data processing
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent segments the complex geochemical data into manageable components through Principal Component Analysis (PCA), which reduces the dimensionality of the dataset. This segmentation allows the system to handle high-vertical resolution measurements efficiently by processing simplified principal components rather than raw multi-element datasets, thereby reducing computational complexity while maintaining accuracy.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent uses automated multivariate statistical algorithms (PCA, HCPC, k-means clustering) to process the high-volume XRF measurement data. These computational methods automatically handle the complexity of analyzing numerous measurements at high resolution, eliminating the need for manual data processing and reducing overall system complexity despite the increased number of measurements.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Facilitates rapid, cost-effective, and accurate stratigraphic zonation and correlation, enhancing reservoir characterization by identifying distinct chemofacies and improving drilling and completion designs, thereby optimizing hydrocarbon recovery.

Implementation Method 1

conducting in-situ high-vertical resolution analyses of the representative core using handheld X-ray fluorescence (HH-XRF), at defined intervals to obtain XRF data

Methodology Applied
Scientific EffectX-ray fluorescence: Fluorescence

Data Source

PatentUS20250377478A1System and method of enhanced stratigraphic zonation and correlation of basinal carbonate mudstone through multivariate statistical analysis
Publication Date: 2025.12.11 KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
  • US20250377478A1 patent drawing
  • US20250377478A1 patent drawing
  • US20250377478A1 patent drawing

AI summary

A system and method for establishing stratigraphic zonation and correlation in basinal mudstone reservoirs including selecting a representative core from wells covering parts of a basin, conducting in-situ high-vertical resolution analyses of the representative core. The high-vertical resolution analysis is conducted using handheld X-ray fluorescence (HH-XRF), at defined intervals to obtain XRF data. In addition, performing PCA and HCPC using the XRF data to generate a plurality of different clusters and validating the different clusters with the representative core to select one cluster. The chemofacies are labeled in the selected cluster using concentrations of three key elements of the different clusters in a ternary diagram. Thereafter, boxplots are generated to determine elements of each chemofacies. Based on that, the distribution of the chemofacies in the well is plotted, and stratigraphic zones are delineated to produce a well-to-well correlation.