Mullite-Talc-Kyanite Composite Containment Element for Ultra-High Pressure

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing containment materials for ultra-high pressure and high temperature applications, such as pyrophyllite, undergo significant phase changes, limiting their suitability and stability under these conditions, and suitable sources are scarce.

Innovation Solution

A pressure containment assembly comprising at least 10 weight percent mullite, 20 weight percent talc, kyanite, a binder material, and up to 15 weight percent silica or glassy phases, with kyanite content at least 5 weight percent, designed to minimize phase changes and maintain mechanical and thermal properties at ultra-high pressures and temperatures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If pyrophyllite is used as containment material for ultra-high pressure applications, then it provides adequate containment capability, but it undergoes significant phase changes at ultra-high pressure and high temperature

Engineering Contradiction:
Improvecontainment capabilityVSAvoidphase change stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent applies composite materials by combining multiple mineral components (mullite, talc, kyanite, silica, and binder materials) in specific weight percentages to create a containment element that maintains structural stability under ultra-high pressure and temperature. This composite approach allows the material to resist phase changes while providing adequate containment capability, directly resolving the contradiction between reliability and compositional stability.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the material composition parameters by specifying precise weight percentages of each component (at least 10% mullite, at least 20% talc, at least 5% kyanite, and controlled silica content) to optimize the phase stability of the containment element under extreme conditions. This parameter optimization ensures the material maintains its structural integrity without undergoing significant phase changes.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If mined pyrophyllite is used for containment vessels, then it provides containment functionality, but suitable sources are limited

Engineering Contradiction:
Improvecontainment functionalityVSAvoidmaterial availability
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent replaces the single-mineral pyrophyllite with a composite material system comprising multiple readily available minerals (mullite, talc, kyanite, silica, and binder materials). This substitution resolves the availability limitation by using common mineral sources while maintaining containment functionality through the synergistic properties of the composite formulation.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the material source strategy from relying on scarce mined pyrophyllite to using abundant mineral components with specified weight percentages. This parameter change in material selection and composition enables widespread availability and adaptability of the containment element while preserving its containment functionality.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If traditional gasket materials are used in high-pressure presses, then they provide sealing capability, but they undergo phase changes that limit their suitability at ultra-high pressure

Engineering Contradiction:
Improvesealing capabilityVSAvoidphase stability under pressure
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent formulates a composite gasket material containing at least 10% mullite, at least 20% talc, at least 5% kyanite, and controlled silica content to maintain phase stability under ultra-high pressure while providing effective sealing. The composite structure prevents harmful phase changes that would otherwise compromise sealing capability in traditional single-mineral materials.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent optimizes the compositional parameters of the gasket material by specifying precise weight percentages of each mineral component. This parameter control ensures the material maintains its sealing capability without undergoing detrimental phase changes at ultra-high pressure, resolving the contradiction between sealing performance and phase stability.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a stable containment element that effectively maintains its properties under extreme conditions, suitable for use in ultra-high pressure and high temperature applications, including the synthesis of super-hard materials, with reduced phase change and enhanced plasticity and machinability.

Implementation Method 1

Pyrophyllite undergoes phase changes at ultra-high pressure and or high temperature. There is a need for containment elements and containment assemblies, particularly but not exclusively for use in containing matter at ultra-high pressure, comprising materials that undergo relatively less phase change at elevated pressure

Methodology Applied
Scientific EffectPhase change resistance: Phase Change

Implementation Method 2

The pressure containment assembly is suitable for containing matter in the solid and or liquid state at an ultra-high pressure at ambient or elevated temperature

Methodology Applied
Scientific EffectPressure transmission: Pressure Increase

Data Source

PatentEP2694453B1Containment element comprising mullite, assembly comprising same, method of making same and method of using same
Publication Date: 2018.07.11 ELEMENT SIX LTD
  • EP2694453B1 patent drawingFigure 1~2

AI summary

A containment element for a pressure containment assembly, comprising mullite or a polymorph of mullite.