Multi-block Olefin Dispersion Heat Resistance

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Solution Overview

Problem

Conventional aqueous dispersions of thermoplastic resins, particularly ethylene copolymers, lack heat resistance and mechanical properties such as compression set, making them unsuitable for applications requiring high heat resistance and durability, like automotive interior components.

Innovation Solution

Development of a catalytic linear multi-block olefin interpolymer dispersion with a combination of hard and soft segments, which includes ethylene/α-olefin or propylene/α-olefin block interpolymers, providing enhanced heat resistance and mechanical properties when used in coatings and foams.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If conventional aqueous dispersions of ethylene copolymers are used, then ease of manufacture and water resistance are achieved, but heat resistance and compression set properties are insufficient

Engineering Contradiction:
Improveheat resistanceVSAvoidcompression set property
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent employs a multi-block copolymer comprising alternating hard segments (high crystallinity, heat resistance) and soft segments (low crystallinity, flexibility). This composite structure at the molecular level allows the material to simultaneously achieve heat resistance from hard segments and maintain compression set properties through soft segments, resolving the contradiction between these two properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The copolymer is segmented into distinct hard and soft blocks along the polymer chain. Hard segments provide thermal stability and structural integrity, while soft segments provide flexibility and resistance to compression set. This segmentation allows each segment to contribute its specific properties, enabling the material to meet both heat resistance and compression set requirements.

Inventive Principle:
Principle #1Segmentation

2Temperature

If homogeneous ethylene-octene copolymers are used for frothed foams, then softness for hygiene applications is achieved, but heat resistance for summer shipment is insufficient

Engineering Contradiction:
Improveheat resistanceVSAvoidmechanical property retention
Core Design Contradiction:
TemperatureVSStrength

Solution Approach 1:

The multi-block copolymer creates a composite structure where hard segments form crystalline regions that maintain mechanical strength at elevated temperatures, while soft segments provide the necessary softness for hygiene applications. This allows the foam to remain soft for comfort while retaining mechanical properties during summer shipment.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

Different regions of the polymer material have different properties: hard segments create localized rigid, heat-resistant zones while soft segments create localized flexible, soft zones. This local quality variation allows the material to exhibit both softness for hygiene applications and heat resistance for summer shipment simultaneously.

Inventive Principle:
Principle #3Local quality

3Adaptability or versatility

If emulsion polymerization process is used, then aqueous dispersion is produced, but the variety of resins is limited and equipment complexity increases

Engineering Contradiction:
Improvevariety of resinsVSAvoidequipment complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent replaces complex chemical polymerization processes with a simpler mechanical mixing approach. Pre-synthesized polyolefin resins are mixed with aqueous dispersing agents using mechanical shear forces, eliminating the need for complex emulsion polymerization equipment and enabling greater resin variety without increasing equipment complexity.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Data Source

PatentEP2041208B1Dispersions of olefin block copolymers
Publication Date: 2017.05.10 DOW GLOBAL TECHNOLOGIES LLC
  • EP2041208B1 patent drawingFigure 1
  • EP2041208B1 patent drawingFigure 2
  • EP2041208B1 patent drawing

AI summary

A dispersion and methods for forming a dispersion that includes a catalytic linear multi-block olefin interpolymer, and at least one dispersing agent, wherein the catalytic linear multi-block olefin interpolymer includes at least one hard segment and at least one soft segment is disclosed. Various applications of the dispersion are also disclosed.