Multi-level Tubular Reactor for Polyester Production

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Solution Overview

Problem

Conventional melt-phase polyester production facilities using mechanically agitated reactors, such as CSTRs, incur high capital, operational, and maintenance costs due to complex and expensive agitators and control equipment, necessitating a more efficient and cost-effective process for producing polyesters like PET.

Innovation Solution

A multi-level tubular reactor configuration featuring a vertically elongated header and horizontally elongated reactor segments, which minimizes mechanical agitation by utilizing flow and gravitational forces to facilitate chemical reactions, allowing for efficient polycondensation of PET with reduced equipment complexity and costs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If mechanically agitated reactors (CSTRs) are used for melt-phase polyester production, then the reaction medium can be thoroughly mixed and controlled, but the capital, operational, and maintenance costs increase due to complex and expensive agitators and control equipment

Engineering Contradiction:
Improvereaction controlVSAvoidagitator and control equipment
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent replaces mechanical agitation systems with a flow-based reactor design where the reaction medium is circulated through tubular reactor segments. The pumping and flow distribution systems replace mechanical agitators, achieving mixing and reaction control through fluid dynamics rather than mechanical motion, thereby reducing device complexity and maintenance requirements

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The reactor is divided into multiple tubular segments arranged in series, with the reaction medium flowing sequentially through each segment. This segmentation allows for staged reaction control and improves heat transfer efficiency while eliminating the need for a single large mechanical agitator, reducing overall system complexity

Inventive Principle:
Principle #1Segmentation

2Stability of the object's composition

If mechanically agitated reactors are used for polyester production, then reaction homogeneity can be maintained, but operational and maintenance expenses increase

Engineering Contradiction:
Improvereaction homogeneityVSAvoidoperational and maintenance expenses
Core Design Contradiction:
Stability of the object's compositionVSEase of operation

Solution Approach 1:

The patent eliminates mechanical agitation by using pumped flow through tubular segments to achieve reaction homogeneity. The circulation system maintains consistent reaction conditions through controlled fluid flow, reducing operational complexity and maintenance expenses associated with mechanical components

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The reactor employs continuous circulation of the reaction medium through the tubular segments, maintaining steady-state flow and reaction conditions. This continuous flow ensures homogeneous reaction composition without requiring mechanical mixing, reducing operational interruptions and maintenance requirements

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration enhances the average chain length of PET production while reducing operational and maintenance expenses, achieving high-efficiency polyester production with minimal mechanical agitation, thus addressing the cost and complexity issues of traditional reactors.

Implementation Method 1

the reaction medium passes downwardly through the header as the reaction medium travels from an upper one of the reactor segments to a lower one of the reactor segments

Methodology Applied
Scientific EffectGravitation: Gravitation

Data Source

PatentUS7847053B2Multi-level tubular reactor with oppositely extending segments
Publication Date: 2010.12.07 ALPEK POLYESTER SA DE CV
  • US7847053B2 patent drawing
  • US7847053B2 patent drawing
  • US7847053B2 patent drawing

AI summary

A multi-level tubular reactor operable to facilitate a chemical reaction in a reaction medium flowing therethrough. The tubular reactor can include a plurality of horizontally elongated and vertically spaced reactor segments coupled to and extending outwardly from a common header. One or more of the reactor segments can contain a tray that divides the internal volume of the reactor segment into upper and lower chambers. The reaction medium can flow away from the header in the upper chambers and back to the header in the lower chambers.