Multi-Port Reaction Vessel Layout for Uniform Hydroxide Precipitation

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Solution Overview

Problem

The production of nickel-containing hydroxide particles in chemical reaction devices requires optimizing the volume fraction of highly supersaturated regions to improve particle quality, as existing methods are device-specific and energy-intensive, leading to inconsistent particle characteristics and increased costs.

Innovation Solution

A chemical reaction device with a design that includes multiple discharge ports and a baffle to reduce the volume fraction of highly supersaturated regions through controlled flow field management, using simulation to determine optimal discharge port placement and agitation conditions, thereby promoting gradual precipitation and improving particle quality.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the volume fraction of highly supersaturated regions is increased to promote particle precipitation, then particle production efficiency is improved, but particle quality deteriorates due to roughness and growth ring-like structures

Engineering Contradiction:
Improveparticle production efficiencyVSAvoidparticle quality
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The invention divides the single discharge port into multiple discharge ports, segmenting the raw material liquid flow into multiple streams. This segmentation reduces the volume fraction of highly supersaturated regions near each discharge port while maintaining overall precipitation efficiency, thereby preventing particle roughness and growth ring structures.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention introduces a baffle to create localized flow patterns that control the distribution of supersaturated regions. The baffle modifies the local flow field to reduce the volume fraction of highly supersaturated regions in specific areas, ensuring uniform particle precipitation and improving particle quality without sacrificing overall productivity.

Inventive Principle:
Principle #3Local quality

2Device complexity

If conventional single discharge port design is used, then device complexity is reduced, but particle quality becomes inconsistent and production efficiency decreases

Engineering Contradiction:
Improvedischarge port configurationVSAvoidparticle characteristic consistency
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The invention segments the discharge port into multiple discharge ports arranged in a specific pattern. This segmentation improves particle characteristic consistency by reducing the volume fraction of highly supersaturated regions, while the modular design maintains reasonable device complexity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The baffle acts as an intermediary element that mediates the flow between the multiple discharge ports and the reaction zone. It controls the flow field to ensure uniform distribution of supersaturated regions, thereby improving particle quality consistency without significantly increasing device complexity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If high agitation speed is used to reduce supersaturated region volume, then particle quality is improved, but energy consumption increases

Engineering Contradiction:
Improveparticle qualityVSAvoidagitation energy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The invention changes the geometric parameters of the discharge ports (number, position, discharge amount) to control the volume fraction of highly supersaturated regions. This parameter optimization achieves particle quality improvement without requiring excessive agitation energy, as the structural design itself contributes to flow control.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The multiple discharge port configuration and baffle design create self-regulating flow patterns that naturally reduce the volume fraction of highly supersaturated regions. The system utilizes the inherent flow dynamics generated by the discharge ports themselves, reducing the need for high-energy agitation while maintaining particle quality.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in consistently high-quality nickel-containing hydroxide particles with reduced roughness and growth ring-like structures, enhancing the efficiency and cost-effectiveness of the particle production process across various device configurations.

Implementation Method 1

supplies a raw material liquid into a solution and causes particles to precipitate in the solution

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 2

optimizing the volume fraction of highly supersaturated regions to improve particle quality

Methodology Applied
Scientific EffectSupersaturation: Supersaturation

Data Source

PatentEP3470136B1Chemical reaction device and particle production method using chemical reaction device
Publication Date: 2024.03.13 SUMITOMO METAL MINING CO LTD
  • EP3470136B1 patent drawingFigure 1
  • EP3470136B1 patent drawingFigure 2
  • EP3470136B1 patent drawingFigure 3

AI summary

A chemical reaction device that supplies a raw material liquid into a solution and causes particles to precipitate in the solution is provided. The chemical reaction device includes an agitation tank configured to accommodate the solution, an impeller configured to agitate the solution, and a plurality of discharge parts configured to discharge the raw material liquid into the solution.