Multi-Stage Chilled Ammonia CO2 Capture System

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Solution Overview

Problem

Current chilled ammonia-based CO2 capture systems for flue gas streams face inefficiencies due to ammonia slip and high operational costs, requiring large absorber vessels and significant refrigeration capacity, which are not effectively addressed by single-stage systems.

Innovation Solution

A multi-stage CO2 capture system using multiple absorber vessels with controlled ionic solution flows and temperatures to minimize ammonia slip, optimizing the ammonia-to-CO2 mole ratio and operating temperatures across different stages for enhanced CO2 capture efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If a single-stage chilled ammonia system is used, then the system structure is simple, but CO2 capture efficiency is low and ammonia slip is high

Engineering Contradiction:
Improvesystem structureVSAvoidCO2 capture efficiency
Core Design Contradiction:
Device complexityVSProductivity

Solution Approach 1:

The absorption process is divided into three distinct stages with different ionic solution temperatures and compositions. The first stage uses a warmer solution for initial CO2 removal, the second stage uses a chilled solution for enhanced capture, and the third stage optimizes for ammonia slip minimization. This segmentation allows each stage to be optimized for its specific function, achieving high overall efficiency while maintaining reasonable system complexity.

Inventive Principle:
Principle #1Segmentation

2Volume of stationary object

If a single-stage chilled ammonia system is used, then the equipment size is small, but significant refrigeration capacity is required

Engineering Contradiction:
Improveabsorber vessel sizeVSAvoidrefrigeration capacity
Core Design Contradiction:
Volume of stationary objectVSUse of energy by stationary object

Solution Approach 1:

The refrigeration load is segmented across three absorption stages, with each stage handling a portion of the CO2 capture at different temperatures. This distributes the refrigeration demand over time and allows heat integration between stages, reducing the peak refrigeration capacity required compared to a single-stage system achieving the same total CO2 removal.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system changes the temperature parameter of the ionic solution across different stages. By using warmer solution in the first stage and progressively colder solution in subsequent stages, the system optimizes the balance between absorption efficiency and refrigeration energy consumption, achieving effective CO2 capture with reduced overall refrigeration capacity requirements.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If ammonia-to-CO2 mole ratio is increased, then CO2 capture efficiency improves, but ammonia slip increases

Engineering Contradiction:
ImproveCO2 capture efficiencyVSAvoidammonia slip
Core Design Contradiction:
ProductivityVSLoss of substance

Solution Approach 1:

The ammonia-to-CO2 mole ratio is optimized differently in each absorption stage. The first stage uses a moderate ratio to achieve initial CO2 removal with minimal ammonia slip, while subsequent stages use progressively optimized ratios to maximize CO2 capture efficiency. This staged optimization allows the system to achieve high overall CO2 removal while minimizing total ammonia slip compared to using a high ratio throughout.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different local conditions (ammonia-to-CO2 mole ratios and temperatures) are applied in different absorption stages to optimize both CO2 capture efficiency and ammonia slip minimization simultaneously, rather than using uniform conditions throughout the system.

Inventive Principle:
Principle #3Local quality

4Ease of manufacture

If operational costs are reduced, then economic viability improves, but CO2 capture efficiency may decrease

Engineering Contradiction:
Improveoperational costsVSAvoidCO2 capture efficiency
Core Design Contradiction:
Ease of manufactureVSProductivity

Solution Approach 1:

The three-stage absorption process segments the CO2 removal task to optimize operational costs. By distributing the capture efficiency requirements across stages with different ionic solution conditions, the system achieves high overall CO2 removal while minimizing the total amount of chilled ionic solution required, thereby reducing energy consumption and operational costs compared to single-stage systems.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The multi-stage system achieves higher CO2 capture efficiency, reduces ammonia slip, and decreases operational costs by optimizing the ammonia-to-CO2 mole ratio and temperature control across stages, allowing for more effective CO2 removal from flue gas streams.

Implementation Method 1

contacting a first ionic solution flow with a flue gas stream to remove a first portion of CO2 from the flue gas stream

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 2

cooling the third ionic solution flow so as to minimize ammonia slip from the ionic solution

Methodology Applied
Scientific EffectCooling: Cooling

Data Source

PatentEP2203240B1Multi-stage co2 removal system and method for processing a flue gas stream
Publication Date: 2012.08.08 ALSTOM TECH LTD
  • EP2203240B1 patent drawingFigure 1A
  • EP2203240B1 patent drawingFigure 1B
  • EP2203240B1 patent drawingFigure 1C

AI summary

An ammonia based CO2 capture system and method is provided in which multiple absorption stages (272, 274 and 276) are provided. Each absorption stage (272, 274 and 276) delivers an ionic solution at a predetermined temperature (T) and contacts it with a flue gas stream (FG).