Multi-Stage Cryogenic Gas Separation for Natural Gas Purification

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current methods for purifying natural gas are often energy inefficient and not feasible for remote locations, failing to effectively remove contaminants like carbon dioxide and NGLs, which reduces the gas value and poses operational challenges.

Innovation Solution

A two-stage process involving cooling and condensation/exchange in separate vessels to remove secondary components and carbon dioxide, combining natural gas sweetening, drying, and NGLs recovery in a single step, reducing energy consumption and equipment size.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If traditional gas separation methods are used, then contaminants can be removed from natural gas, but energy consumption increases and extraction capacity is limited

Engineering Contradiction:
Improveenergy consumptionVSAvoidextraction capacity
Core Design Contradiction:
Loss of energyVSProductivity

Solution Approach 1:

The gas separation process is divided into multiple stages with different cooling temperatures. The first stage removes heavier components at higher temperatures, while subsequent stages remove lighter components at progressively lower temperatures. This segmented approach optimizes energy usage by not cooling the entire gas stream to the lowest temperature required, thereby reducing overall energy consumption while maintaining high extraction capacity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention changes the temperature parameter progressively through multiple separation stages. By adjusting the cooling temperature at each stage according to the specific components being removed, the process achieves efficient separation with reduced energy input compared to single-stage low-temperature separation, thus resolving the contradiction between energy loss and productivity.

Inventive Principle:
Principle #35Parameter changes

2Device complexity

If multiple treatment steps are integrated into a single process, then capital costs and equipment size decrease, but process complexity increases

Engineering Contradiction:
Improveequipment sizeVSAvoidprocess integration
Core Design Contradiction:
Device complexityVSEase of manufacture

Solution Approach 1:

The invention combines multiple gas treatment functions (dehydration, NGL recovery, CO2 removal, and natural gas liquefaction) into a single integrated process flow. By merging these previously separate treatment steps into one continuous process with sequential cooling stages, the total equipment size and capital costs are reduced while the manufacturing complexity is managed through standardized modular design.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The separation system performs multiple functions simultaneously: it dehydrates natural gas, recovers NGLs, removes CO2, and produces liquid natural gas. This multi-functional approach eliminates the need for separate dedicated equipment for each treatment step, thereby reducing overall device complexity and capital investment while maintaining ease of manufacture through a unified process design.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Manufacturing precision

If natural gas is cooled to remove contaminants, then purification efficiency increases, but methane condensation losses increase

Engineering Contradiction:
Improvepurification efficiencyVSAvoidmethane condensation losses
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The invention applies different cooling temperatures to different portions of the gas stream at different stages. Rather than uniformly cooling the entire stream to the lowest temperature, each stage uses the minimum necessary temperature to remove specific contaminants. This localized temperature application maximizes purification efficiency for each component while minimizing unnecessary methane condensation and associated losses.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The process removes contaminants in multiple partial stages rather than attempting complete removal in a single low-temperature stage. Each stage removes a portion of the contaminants at progressively lower temperatures, achieving high overall purification efficiency while avoiding excessive methane condensation that would occur in a single extreme low-temperature step.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances NGLs recovery, reduces energy consumption, eliminates chemical hazards, and decreases capital costs by integrating multiple treatment steps into a single process, making it more efficient and cost-effective for natural gas purification.

Implementation Method 1

A first portion of the secondary component condenses, desublimates, or a combination thereof

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 2

A first portion of the secondary component condenses, desublimates, or a combination thereof

Methodology Applied
Scientific EffectDesublimation: Sublimation

Implementation Method 3

a first portion of the methane condenses as a first liquid methane stream

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 4

a first portion of the carbon dioxide desublimates to form a solid product stream

Methodology Applied
Scientific EffectDesublimation: Sublimation

Data Source

PatentUS10995984B2Method for separating components of a gas
Publication Date: 2021.05.04 U S BANK TRUST CO NAT ASSOC
  • US10995984B2 patent drawing
  • US10995984B2 patent drawing
  • US10995984B2 patent drawing

AI summary

A method is disclosed for separating components of a gas. A feed gas stream is cooled in the first vessel. The feed gas stream comprises methane, carbon dioxide, and a secondary component. A first portion of the secondary component condenses, desublimates, or a combination thereof to form a primary stream, resulting in a first depleted gas stream. The first depleted gas stream is cooled in a condensing exchanger such that a first portion of the methane condenses as a first liquid methane stream, resulting in a second depleted gas stream. The second depleted gas stream is cooled in the second vessel such that a first portion of the carbon dioxide desublimates to form a solid product stream, resulting in a third depleted gas stream.