Multi-Stage Glass Tempering with Varying Heat Transfer Rates

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Solution Overview

Problem

Conventional thermal tempering processes are limited in achieving high surface compression and center tension in glass sheets, which restricts the production of highly tempered glass suitable for applications like hurricane-resistant windows and aircraft glass, due to processing methods that do not allow for sufficient heat transfer optimization.

Innovation Solution

A multi-stage tempering process involving quench stations with varying heat transfer rates, where the glass is initially cooled at a first heat transfer rate and then at a higher rate at subsequent stations, allowing for increased surface compression and center tension without causing glass breakage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If conventional single-stage thermal tempering is used, then the glass achieves basic tempering with moderate surface compression and center tension, but the tempering level is limited and insufficient for high-strength applications like hurricane-resistant windows

Engineering Contradiction:
Improvesurface compression and center tensionVSAvoidtempering process complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The tempering process is divided into multiple sequential quenching stages, each with different heat transfer rates. The glass sheet passes through several quenching zones where the heat transfer coefficient is progressively increased, allowing the surface compression and center tension to be built up in stages rather than all at once, thereby achieving high tempering levels without excessive process complexity

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The heat transfer rate parameter is systematically varied across different quenching stages. By increasing the heat transfer coefficient from the first quenching stage to subsequent stages, the process optimizes the development of surface compression and center tension, enabling high-strength tempering that cannot be achieved with constant heat transfer rates

Inventive Principle:
Principle #35Parameter changes

2Strength

If higher heat transfer rates are applied throughout the entire tempering process, then higher tempering levels are achieved, but glass breakage increases due to excessive thermal stress

Engineering Contradiction:
Improvetempering levelVSAvoidglass breakage
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The first quenching stage applies a moderate heat transfer rate to initially cool the glass surface and establish a controlled thermal gradient. This preliminary action prepares the glass for subsequent higher-rate quenching by reducing the temperature differential gradually, preventing excessive thermal stress that would cause breakage

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The heat transfer rate is made dynamic rather than static, progressively increasing from the first quenching stage to subsequent stages. This dynamic adjustment allows the process to adapt to the changing thermal state of the glass, applying higher cooling rates only when the glass can withstand them, thereby maximizing tempering level while minimizing breakage

Inventive Principle:
Principle #15Dynamics

3Strength

If multi-stage quenching with varying heat transfer rates is implemented, then significantly higher tempering levels are achieved, but the process complexity and equipment requirements increase

Engineering Contradiction:
Improvesurface compression and center tensionVSAvoidquenching system complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The quenching system is segmented into multiple independent zones, each capable of delivering a specific heat transfer rate. This segmentation allows the complex tempering profile to be achieved through simpler, modular zones rather than requiring a single complex system, making the increased complexity manageable and implementable

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process achieves significantly higher tempering levels than conventional methods, producing glass with enhanced strength and fracture resistance suitable for demanding applications while minimizing breakage and maintaining optical quality.

Implementation Method 1

cooling the glass sheet at a first heat transfer rate, e.g., using a first heat transfer coefficient, at a first quench station, and cooling the glass sheet at a second heat transfer rate at a second quench station

Methodology Applied
Scientific EffectHeat transfer: Conduction (thermal)

Implementation Method 2

glass sheets are heated to an elevated temperature above the glass strain point near the glass softening point and then are chilled to cool the glass surface regions relatively rapidly while the inner regions of the glass cool at a slower rate

Methodology Applied
Scientific EffectThermal tempering: Thermal Shock

Data Source

PatentEP1957419B1Apparatus and method for tempering glass sheets
Publication Date: 2018.07.04 VITRO
  • EP1957419B1 patent drawingFigure 1
  • EP1957419B1 patent drawingFigure 2
  • EP1957419B1 patent drawingFigure 3

AI summary

A method of tempering a glass sheet heated to a tempering temperature includes cooling the glass sheet at a first heat transfer coefficient at a first quench station and cooling the glass sheet at a second heat transfer coefficient at a second quench station downstream of the first quench station. The second heat transfer coefficient is greater than the first heat transfer coefficient. In a multistage process of the invention, a plurality of quench stations could be used with each downstream quench station having a larger heat transfer coefficient than the previous upstream quench station.