Multilayer Coating System for Aerospace Substrates

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Solution Overview

Problem

Conventional basecoat/clearcoat systems are not well-suited for aerospace applications due to the flexibility requirements of aluminum substrates and exposure to extreme temperature variations, high winds, and corrosive substances, while also needing a balance between long pot-life and fast dry times to ensure intercoat adhesion.

Innovation Solution

A multilayer, ambient cure coating system comprising a 2K polyurethane basecoat and clearcoat composition with a low Tg branched polyester polyol and high Tg thermoplastic resin, allowing for excellent intercoat and substrate adhesion, solvent, and water resistance, even when the clearcoat is applied up to 72 hours after the basecoat, with a catalyst like dibutyltin dilaurate for isocyanate crosslinking.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional basecoat/clearcoat systems are used, then the coating can be applied quickly, but the coating lacks flexibility and adhesion to aluminum substrates under extreme aerospace conditions

Engineering Contradiction:
Improvecoating adhesion and flexibilityVSAvoidsuitability for aerospace conditions
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent modifies the chemical parameters of the polyol component by incorporating specific ratios of polycaprolactone (providing flexibility and low Tg) and aromatic polyols (providing strength and high Tg). This parameter adjustment allows the coating to maintain both flexibility and adhesion under extreme aerospace conditions including temperature variations from -50°C to over 60°C and exposure to corrosive substances.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses a composite polyol system combining multiple polyol types (polycaprolactone, aromatic polyols, and additional polyols) to create a binder that simultaneously provides flexibility, adhesion, and resistance to extreme conditions. This composite approach allows the coating to meet the demanding requirements of aerospace applications that single-component systems cannot satisfy.

Inventive Principle:
Principle #40Composite materials

2Productivity

If the coating is formulated to dry quickly, then subsequent layers can be applied faster, but intercoat adhesion deteriorates due to premature vitrification

Engineering Contradiction:
Improvecoating application speedVSAvoidintercoat adhesion
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent creates a dynamic curing system where the polyol composition enables the coating to progress through different stages: initial flexibility for application, controlled gelation for intercoat bonding, and final cure for performance. The specific polyol blend allows workers to apply subsequent layers within a extended window (up to 72 hours) while maintaining excellent intercoat adhesion, as the coating remains sufficiently reactive without premature vitrification.

Inventive Principle:
Principle #15Dynamics

3Duration of action of moving object

If the coating pot-life is extended for large substrate coating, then the coating remains workable longer, but the overall cure rate decreases

Engineering Contradiction:
Improvepot-lifeVSAvoidcure rate
Core Design Contradiction:
Duration of action of moving objectVSSpeed

Solution Approach 1:

The invention implements a multi-stage curing process through its polyol formulation. The coating progresses through distinct phases: an extended open pot-life period allowing workability for large substrates, followed by a gelation phase, and finally a cure phase. The specific polyol composition (combining polycaprolactone, aromatic polyols, and additional polyols) enables this periodic action, providing both extended pot-life for large aircraft surfaces and adequate cure rate for performance.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system provides excellent overall performance with balanced flexibility and cure rate, ensuring intercoat adhesion and resistance to extreme conditions, making it suitable for large aerospace substrates.

Implementation Method 1

an isocyanate functional material suitable for crosslinking the polyester polyol

Methodology Applied
Scientific EffectIsocyanate crosslinking: Chemical Bonding

Implementation Method 2

A low Tg branched polyester polyol having a Tg of between -40°C to 20°C

Methodology Applied
Scientific EffectGlass transition temperature effect:

Implementation Method 3

which is the esterification reaction product of a monomer blend comprising

Methodology Applied
Scientific EffectEsterification reaction: Chemical Bonding

Data Source

PatentEP2396123B1Compositions for multilayer coating and resins therefore
Publication Date: 2015.06.03 SHERWIN WILLIAMS LUXEMBOURG INVESTMENT MANAGEMENT

AI summary

A 2K basecoat clearcoat system includes a solvent borne basecoat having a low Tg branched polyester polyol, optionally, a high Tg, high molecular weight thermoplastic resin, and a hardener that includes an isocyanate functional material suitable for crosslinking the polyester polyol, and optional thermoplastic resin. The solvent borne clearcoat composition includes a low Tg linear or branched polyester polyol, at least one other multi-functional polyol, and an isocyanate functional material suitable for crosslinking the polyester and multi-functional polyols.