Multilayer Flexible Packaging with Core-Shell Antioxidant Capsules

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Solution Overview

Problem

Existing methods for integrating antioxidants into packaging materials face limitations such as reduced effectiveness due to distance from the outer layer, instability at high temperatures, and incompatibility with polymers, leading to reduced antioxidant activity and limited applications.

Innovation Solution

A multilayered flexible package with core-shell antioxidant capsules, sized between 0.1 and 10 µm, encapsulated in a polymeric shell, dispersed in a polymeric coating, providing a 0.1 to 0.5 V reduction potential, enhances antioxidant protection and homogeneity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If antioxidants are added as solid, liquid, oil, powder or emulsion into polymeric material during extrusion, then antioxidant species are integrated into the packaging material, but the layer thickness becomes at least 100-200 μm which reduces possible applications

Engineering Contradiction:
Improveantioxidant integrationVSAvoidlayer thickness
Core Design Contradiction:
Quantity of substanceVSLength of stationary object

Solution Approach 1:

The patent changes the physical state parameter of the antioxidant from bulk (solid/liquid) to nanoscale particles (1-100 nm), enabling integration into thin polymer layers while maintaining sufficient antioxidant quantity and activity

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses thin polymeric films (can be less than 100 μm) containing nanoscale antioxidant particles, allowing the packaging to achieve both adequate antioxidant content and reduced thickness for various applications

Inventive Principle:
Principle #30Flexible shells and thin films

2Quantity of substance

If antioxidants are placed deep within the polymer layer, then antioxidant species are integrated into the package structure, but the distance from the outer portion reduces antioxidant activity

Engineering Contradiction:
Improveantioxidant integrationVSAvoidantioxidant activity
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent changes the size parameter of antioxidant particles to nanoscale (1-100 nm), enabling them to be uniformly distributed throughout the thin polymer layer and positioned close to the outer surface, thereby maintaining high antioxidant activity while ensuring deep integration

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a nanoscale dispersed system where antioxidant particles are distributed throughout the polymer matrix, creating a effectively porous structure at nanoscale that allows antioxidant molecules to reach the outer surface efficiently

Inventive Principle:
Principle #31Porous materials

3Ease of manufacture

If elevated temperatures are applied during extrusion process, then polymeric material is processed and formed, but antioxidant molecules undergo spoilage and degradation

Engineering Contradiction:
Improvepolymer processingVSAvoidantioxidant stability
Core Design Contradiction:
Ease of manufactureVSStability of the object's composition

Solution Approach 1:

The patent changes the size parameter of antioxidant particles to nanoscale (1-100 nm), which increases their surface area to volume ratio and enhances their stability against thermal degradation during processing while maintaining processing feasibility

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite material system where nanoscale antioxidant particles are dispersed in the polymer matrix, combining the processing properties of the polymer with the thermal stability and antioxidant properties of the nanoparticles

Inventive Principle:
Principle #40Composite materials

4Reliability

If specific antioxidant molecules such as catechines are integrated into polymer, then antioxidant protection is provided, but distribution and effectiveness are strictly related to chemical compatibility with the polymer

Engineering Contradiction:
Improveantioxidant protectionVSAvoidpolymer compatibility
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent changes the size parameter of antioxidant particles to nanoscale (1-100 nm), which improves their dispersion and compatibility with various polymer matrices regardless of the specific chemical nature of the antioxidant molecule, thereby increasing versatility across different polymer types

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The core-shell structure maintains antioxidant effectiveness by preventing degradation and ensures uniform distribution, extending the preservation time of air-sensitive materials.

Implementation Method 1

the oxidation process is considered the major cause of deterioration for perishable goods and foods affecting their quality and safety

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 2

a core-shell system dispersion... comprising a core of an antioxidant with a reduction potential comprised between 0.1 and 0.5 V, and a polymeric shell covering the core at least by 70%

Methodology Applied
Scientific EffectEncapsulation: Physical Containment

Data Source

PatentEP4077526B1Multilayered flexible package with antioxidant properties
Publication Date: 2025.10.01 SAES GETTERS SPA
  • EP4077526B1 patent drawingFigure 1~2
  • EP4077526B1 patent drawingFigure 3A
  • EP4077526B1 patent drawingFigure 3B

AI summary

A multilayered flexible package comprises a polymeric coating (2) that contains a dispersion of antioxidant capsules (3) having a particle size distribution comprised between 0.1 and 10 µm and a core-shell structure comprising a core (4), of an antioxidant with a reduction potential comprised between 0.1 and 0.5 V, and a polymeric shell (5) covering the core (4) at least by 70%.