Multivitamin Tablet Stability via Anhydrous Dicalcium Phosphate

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Solution Overview

Problem

Multivitamin and mineral supplements experience degradation and discoloration due to oxidation reactions, particularly caused by moisture, leading to reduced potency and unappealing darkening or spotting, which conventional desiccants and coatings fail to adequately address.

Innovation Solution

A pharmaceutical composition comprising at least one polyvalent metal and one oxidizable vitamin, combined with anhydrous dicalcium phosphate to minimize mobile bound water, thereby reducing oxidation-induced spotting and darkening, and maintaining the stability and disintegration time of multivitamin and mineral supplements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If desiccants are employed to remove moisture, then stability against oxidation is improved, but desiccants can be physically removed by consumers negating the beneficial effect

Engineering Contradiction:
Improvestability against oxidationVSAvoidconsumer removal of desiccant
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent extracts the harmful moisture from the system by incorporating water-binding materials directly into the tablet matrix, eliminating the need for separate desiccant packets that can be removed by consumers. The water-binding capacity is built into the excipients themselves.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

Water-binding materials serve as intermediaries that bind moisture within the tablet structure, preventing direct contact between water and oxidizable components. This internal moisture management system replaces external desiccants.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If desiccants are used to control moisture, then oxidation degradation is reduced, but desiccants add expense to the final product

Engineering Contradiction:
Improvereduction of oxidation degradationVSAvoidproduct cost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent uses excipients that serve multiple functions: they act as fillers, binders, and water-binding agents simultaneously. This eliminates the need for separate desiccant components, reducing overall product cost while maintaining stability.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The tablet formulation itself provides moisture control through water-binding excipients integrated into the matrix, making the system self-regulating without requiring additional moisture-control components that would increase cost.

Inventive Principle:
Principle #25Self-service

3Ease of operation

If tablet coating is employed to limit exposure to environmental water, then consumer perception of spotting is improved, but coating does not appreciably reduce spotting and darkening problems

Engineering Contradiction:
Improveconsumer perceptionVSAvoidreduction of spotting and darkening
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent addresses moisture control and oxidation prevention during the tablet formulation stage by incorporating water-binding excipients and antioxidants into the matrix, preventing degradation before it occurs rather than merely masking it with coating.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent changes the chemical environment within the tablet by using water-binding excipients that alter moisture availability, and by selecting antioxidants that change the oxidation resistance parameters of the formulation, addressing the root cause rather than symptoms.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If water-binding materials are incorporated into the tablet matrix, then oxidation reactions are reduced, but tablet formulation complexity increases

Engineering Contradiction:
Improvereduction of oxidation reactionsVSAvoidtablet formulation complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent selects excipients that perform multiple functions simultaneously: water binding, filling, binding, and disintegration. This multi-functionality approach maintains formulation simplicity while achieving moisture control and oxidation prevention.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent modifies existing excipient selection criteria to prioritize water-binding capacity and oxidation resistance, changing the formulation parameters to inherently more stable materials rather than adding complex moisture-control systems.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition significantly improves chemical stability, maintains potency, and prevents spotting and darkening over the commercial shelf life of multivitamin and mineral supplements, ensuring consistent disintegration times and enhanced stability.

Implementation Method 1

The water that contributes to degradation is bound water within the tablet matrix... The present invention provides a composition and method to reduce the degradation in vitamin and mineral supplements associated with darkening and/or spotting... comprising anhydrous dicalcium phosphate

Methodology Applied
Scientific EffectWater binding: Absorption (physical)

Implementation Method 2

The most common of these reactions are degradation reactions that lead to a reduced potency of the impacted nutrients and may also cause the composition to darken or develop unsightly dark spots. Oxidation reactions are exemplary of a common form of degradation reactions.

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentEP2111126B1Improved stability in vitamin and mineral supplements
Publication Date: 2013.11.13 WYETH LLC

AI summary

The invention provides a multivitamin and mineral nutritional supplement composition comprising at least one polyvalent metal and at least one oxidizable vitamin with substantially improved resistance to reactions that lead to darkening and /or spotting and reactions that may reduce the potency of oxidizable vitamins. The composition is a multivitamin and mineral composition comprising at least one polyvalent metal and at least one oxidizable vitamin wherein the composition is substantially free of mobile bound water. The invention also includes methods for making such a composition and methods of preventing or reducing oxidation, improving the stability of oxidizable vitamins, and stabilizing the disintegration time of a multi-vitamin and mineral nutritional supplement composition.