Multi-well plate insert with flat electrodes for impedance measurement

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Solution Overview

Problem

Existing multi-well plate systems for measuring cellular and trans-cellular impedance are prone to electrode damage, inconsistent electrode positioning, and liquid level variations, leading to inaccurate and invasive measurements of biological barrier integrity.

Innovation Solution

A multi-well plate system with electrodes integrated into the well insert, arranged flat along the surface to prevent bending and ensure consistent positioning, and a four-terminal measurement system for precise impedance analysis, minimizing the risk of damage and ensuring reproducibility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If electrodes are arranged to project into the liquid in the well insert, then electrical contact with the conductive medium is ensured, but the electrodes are susceptible to damage and may contact or damage the cell layer

Engineering Contradiction:
Improveelectrode contact reliabilityVSAvoidcell layer damage
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The electrodes are arranged flat along the surface of the well insert rather than projecting vertically into the liquid. This dimensional change from vertical projection to horizontal surface arrangement ensures electrical contact with the conductive medium while eliminating the risk of electrodes contacting or damaging the cell layer grown on the membrane.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Reliability

If electrodes are arranged to project into the liquid in the well insert, then electrical contact is achieved, but the electrodes can be bent or broken easily

Engineering Contradiction:
Improveelectrode contact reliabilityVSAvoidelectrode mechanical strength
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The electrodes are configured as flat surfaces arranged along the well insert surface rather than protruding elements. This dimensional reconfiguration eliminates the mechanical vulnerability of protruding electrodes to bending or breaking while maintaining effective electrical contact with the conductive medium through the liquid medium.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Adaptability or versatility

If electrodes are positioned in different components of the device, then assembly flexibility is provided, but inconsistent positioning and measurement variability occur

Engineering Contradiction:
Improveassembly flexibilityVSAvoidimpedance measurement consistency
Core Design Contradiction:
Adaptability or versatilityVSMeasurement precision

Solution Approach 1:

The electrodes are integrated into the well insert as a single unified component rather than being distributed across separate components. This merging ensures consistent and reproducible electrode positioning for all measurements while maintaining assembly flexibility, as the integrated electrodes move with the well insert as one unit.

Inventive Principle:
Principle #5Merging (Combining)

4Ease of operation

If simple microscopic observation is used to determine cell layer integrity, then the method is simple and redundant control is provided, but accuracy and sensitivity are insufficient

Engineering Contradiction:
Improvemeasurement simplicityVSAvoidcell layer integrity accuracy
Core Design Contradiction:
Ease of operationVSMeasurement precision

Solution Approach 1:

The patent introduces an electrical impedance measurement system as an intermediary method between simple microscopic observation and complex electrochemical methods. This intermediary approach uses electrical properties to accurately and sensitively assess cell layer integrity and barrier function, providing quantitative data that bridges the gap between visual inspection and sophisticated electrochemical analysis.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system provides accurate, non-invasive, and reproducible measurements of biological barrier integrity by ensuring electrodes are always submerged in the liquid and maintaining consistent positioning, reducing the risk of damage and variability in results.

Implementation Method 1

The electrical resistance, and more generally the impedance across a cell monolayer or multiple layers of cells is a measure of its ion permeability and thus a very useful parameter to determine properties of the biological barrier

Methodology Applied
Scientific EffectElectrical impedance: Electrical Resistance

Implementation Method 2

Impedance spectroscopy, using a number of defined frequencies, has proved particularly powerful for this purpose. Different from other electrochemical methods, which only work with direct current (DC) voltage or alternating current (AC) voltage with constant frequency, impedance spectroscopy uses AC voltage with sinusoidal, square or triangular waveform frequency, which varies during the measurement

Methodology Applied
Scientific EffectImpedance spectroscopy:

Data Source

PatentEP4317397A1Multi-well plate system for assessing cell layers
Publication Date: 2024.02.07 SIMPLINEXT SA
  • EP4317397A1 patent drawingFigure 1a~1b
  • EP4317397A1 patent drawingFigure 2a~2c
  • EP4317397A1 patent drawingFigure 3a~3b

AI summary

The invention concerns a well insert (1) for a multi-well plate (2) and a multi-well plate system for use in cell culture. The well insert comprises a planar support (14) having at least one permeable or semi-permeable portion (11), at least one pair of electrodes having a first electrode (41) and a second electrode (42) arranged to measure electrical impedance across a layered cell culture supported by the planar support (14), an insert wall with a projecting portion (13), said projecting portion being configured to interface with the multi-well plate (2) such as to suspend the insert (1) in a well (20), wherein the insert wall (12) together with the planar support (14) separate a first chamber (8) from a second chamber (9), the electrodes (41, 42) being arranged along the inner surface (15) of the insert and the counter-electrode (41, 42) being arranged along the outer surface (16) of the insert. The projecting portion (13) comprises the contact ends (53, 54) of the one or more electrode and of the one or more counter-electrode, such that each electrode connects to a contact point (45) on the multi-well plate 2 and each counter-electrode connects to a contact point (35) on the lid (3), which is positioned on the plate (2) when the system is assembled.