3D Nano-Shell Micro Pre-Concentrator for Uniform Gas Desorption

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Solution Overview

Problem

Conventional micro pre-concentrators face challenges in efficiently concentrating gaseous components with low concentration due to random porous structures that hinder smooth gas flow and uniform heating, leading to reduced concentration performance.

Innovation Solution

A micro pre-concentrator with a 3D nano-shell composite structure, comprising a ceramic-polymer composite with ordered pores and a thin film support, is developed, featuring a large surface area and uniform heat transfer, enhancing gas absorption and desorption efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Area of stationary object

If a random porous structure with micron scale is used, then the specific surface area is large, but gaseous molecules cannot flow smoothly and heat cannot be provided uniformly

Engineering Contradiction:
Improvespecific surface areaVSAvoidgas flow smoothness
Core Design Contradiction:
Area of stationary objectVSEase of operation

Solution Approach 1:

The patent employs a porous polymer material with controlled pore structure to create the coating layer. The porous structure provides large specific surface area for gas absorption while maintaining interconnected pores that enable smooth gas flow throughout the material, resolving the contradiction between surface area and flow smoothness.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent creates a composite structure by coating porous polymer material onto the inner surface of the micro-column. This composite approach combines the large surface area advantage of porous materials with the structural integrity needed for uniform heat distribution, allowing both high surface area and smooth gas flow to coexist.

Inventive Principle:
Principle #40Composite materials

2Area of stationary object

If a random porous structure with micron scale is used, then the specific surface area is large, but heat cannot be provided uniformly leading to desorption failure

Engineering Contradiction:
Improvespecific surface areaVSAvoidheat uniformity
Core Design Contradiction:
Area of stationary objectVSTemperature

Solution Approach 1:

The porous polymer coating layer with its interconnected pore structure enables uniform heat distribution throughout the material. The porous structure allows heat to penetrate evenly across the entire surface area, preventing localized hot or cold spots that would cause desorption failure, while maintaining the large surface area needed for effective gas concentration.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent applies a coating layer with specific local properties (porous polymer material) to the inner surface of the micro-column. This localized application ensures that the heat transfer properties are optimized at the gas-contact interface, providing uniform heat distribution exactly where needed for consistent desorption performance across the entire surface area.

Inventive Principle:
Principle #3Local quality

3Productivity

If a conventional porous structure is used, then absorption/desorption efficiency is maximized, but desorption failure occurs due to non-uniform heating

Engineering Contradiction:
Improveabsorption/desorption efficiencyVSAvoiddesorption consistency
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The porous polymer coating layer maintains high absorption/desorption efficiency through its large surface area and porous structure, while simultaneously ensuring uniform heat distribution throughout the material. This uniform heating prevents localized desorption failures, thereby improving the reliability and consistency of the desorption process without sacrificing productivity.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The composite structure of porous polymer coating on the micro-column interior combines the high surface area benefits for efficient absorption/desorption with the thermal properties needed for uniform heating. This composite approach resolves the contradiction between productivity and reliability by ensuring both efficient mass transfer and consistent thermal treatment across the entire adsorbent material.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The 3D nano-shell composite structure increases the adsorption capacity and concentration performance by allowing uniform and rapid heat transfer, enabling high-density gas release and improved detection of volatile organic compounds.

Implementation Method 1

The 3D nano-shell composite structure increases the adsorption capacity and concentration performance by allowing uniform and rapid heat transfer

Methodology Applied
Scientific EffectHeat transfer: Conduction (thermal)

Implementation Method 2

a 3D nano-shell composite disposed in the trench and having pores that are ordered and connected to each other... enhancing gas absorption and desorption efficiency

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

The micro pre-concentrator further includes a heating member disposed under the base substrate

Methodology Applied
Scientific EffectHeating: Heating

Data Source

PatentUS20230341302A1Micro pre-concentrator having ceramic-polymer composite with 3D NANO-shell structure and method for manufacturing the same
Publication Date: 2023.10.26 KOREA ADVANCED INST OF SCI & TECH
  • US20230341302A1 patent drawing
  • US20230341302A1 patent drawing
  • US20230341302A1 patent drawing

AI summary

A disclosed micro pre-concentrator includes a base substrate having a trench, and a 3D nano-shell composite disposed in the trench and having pores that are ordered and connected to each other. The 3D nano-shell composite includes a 3D nano-shell support defined by a thin film extending three-dimensionally and a polymeric layer formed along a surface of the 3D nano-shell support. The micro pre-concentrator may increase adsorption amount of gas. In addition, since it may be uniformly heated in a short time, it is possible to release gas at a high density in a short time.