Nanoparticle Size Uniformity via Gradient Electromagnetic Field

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Solution Overview

Problem

Current methods lack the capability to produce high volume, uniformly sized, ionically stable nanoparticles, particularly spherical nanoparticles, that can be suspended in liquid solutions without the need for surfactants or stabilizing agents.

Innovation Solution

The process involves ablation of a target surface using specific energy packets to create an ejecta event, followed by the application of a gradient electromagnetic field to achieve uniform particle size and shape, ensuring stability and suspension in liquid media without the use of surfactants. This method utilizes laser ablation or electrical discharge to produce spherical nanoparticles from various materials, including metals and nonmetallic substances.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If traditional nanoparticle production methods are used, then nanoparticles can be created, but they exhibit non-uniform size distribution and require surfactants for stabilization

Engineering Contradiction:
Improvenanoparticle size uniformityVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent applies parameter changes by precisely controlling laser pulse duration (picosecond range), energy density, and pulse frequency to achieve uniform nanoparticle sizes without surfactants. The specific parameter range of 1-100 picoseconds for pulse duration and controlled energy density are critical for producing monodisperse particles

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs periodic pulsed laser ablation where multiple pulses are delivered in sequence with controlled intervals. This periodic action allows cumulative energy deposition that progressively refines particle size uniformity while preventing aggregation, eliminating the need for stabilizing agents

Inventive Principle:
Principle #19Periodic action

2Productivity

If laser ablation is used to produce nanoparticles, then particles can be created, but the production volume is limited

Engineering Contradiction:
Improvenanoparticle production volumeVSAvoidnanoparticle size uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent implements continuous pulsed laser ablation where pulses are delivered continuously over an extended period rather than as single shots. This continuous action enables accumulation of large quantities of nanoparticles while maintaining size uniformity through consistent energy deposition parameters across all pulses

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent makes the laser ablation system multi-functional by adjusting pulse parameters to simultaneously achieve high production volume and uniform particle sizes. The same apparatus can produce different quantities of particles by simply modifying pulse frequency and duration without sacrificing size control

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Manufacturing precision

If non-spherical nanoparticles are produced through chemical reduction, then size control is good, but further processing is required to achieve spherical shapes

Engineering Contradiction:
Improvenanoparticle size controlVSAvoidmanufacturing simplicity
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent performs preliminary shaping during the ablation process itself by controlling laser parameters to directly produce spherical particles from the target material. This preliminary action eliminates the need for subsequent milling or reshaping steps that would be required if non-spherical particles were produced first

Inventive Principle:
Principle #10Preliminary action

4Stability of the object's composition

If surfactants are used to stabilize nanoparticles in solution, then particles remain suspended, but surfactants cause problems in biological and other sensitive applications

Engineering Contradiction:
Improvenanoparticle suspension stabilityVSAvoidsurfactant interference
Core Design Contradiction:
Stability of the object's compositionVSObject-affected harmful factors

Solution Approach 1:

The patent extracts and eliminates the need for surfactants by producing nanoparticles with inherent stability through precise laser ablation parameters. The particles are produced with surface characteristics that naturally prevent aggregation, removing the harmful surfactant component entirely from the system

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The nanoparticles produced by this method are self-stabilizing in solution without requiring external surfactants. The laser ablation process imparts surface properties to the particles that enable them to maintain suspension stability autonomously, making the system self-sufficient

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process results in nanoparticles with uniform size distribution, high stability, and the ability to remain suspended in polar liquids without surfactants, enabling their use in applications where surfactants would be problematic, such as biological systems.

Implementation Method 1

Ablation of a target surface with discrete energy packets delivered by a laser or other means to create an ejecta event

Methodology Applied
Scientific EffectLaser ablation: Laser Ablation

Implementation Method 2

Application of a gradient electromagnetic field to the ejecta event to uniformize the size and shape of the particles

Methodology Applied
Scientific EffectElectromagnetic field: Electromagnetic Induction

Data Source

PatentUS10610934B2Method and apparatus for production of uniformly sized nanoparticles
Publication Date: 2020.04.07 EVOQ NANO INC
  • US10610934B2 patent drawing
  • US10610934B2 patent drawing
  • US10610934B2 patent drawing

AI summary

An apparatus and process for creating uniformly sized, spherical nanoparticles from a solid target. The solid target surface is ablated to create an ejecta event containing nanoparticles moving away from the target surface. Ablation may be performed by laser or electrostatic discharge. At least one continuous planar electromagnetic field is placed in front of the solid target surface being ablated. The electromagnetic field manipulates at least a portion of the nanoparticles as they move away from the target surface and pass through the electromagnetic field to increase size and spherical shape uniformity of the nanoparticles. The manipulated nanoparticles are collected as a stable suspension in a fluid.