Nanoporous Coated FBG Sensor for High-Temperature Gas Detection

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Solution Overview

Problem

Current optical sensors based on fibre Bragg gratings face limitations in extreme conditions such as high temperature and pressure, particularly in underground oil and gas reservoirs, with issues like long response times, hysteresis effects, and limited durability, as well as a need for improved selectivity, accuracy, and robustness for detecting compounds like alkanes and alkanols.

Innovation Solution

A waveguide with a Fibre Bragg Grating coated using a nanoporous sensor material, such as zeolites or metal-organic frameworks, which absorbs analytes without causing significant temperature changes, allowing for continuous, non-destructive detection with enhanced sensitivity and stability under extreme conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If organic polymer coatings (polyacrylate, polyimide) are used on FBG to detect gas concentrations, then the sensor can measure humidity and CO2 levels, but the sensor usability is limited at elevated temperatures

Engineering Contradiction:
Improvesensor usability at elevated temperaturesVSAvoidtemperature range for operation
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent changes the material parameter of the coating from organic polymers to inorganic nanoporous materials (zeolites, metal oxides), which fundamentally alters the temperature stability characteristics and enables operation at elevated temperatures while maintaining sensing functionality

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite structures combining FBG waveguides with nanoporous sensor material coatings, creating a hybrid system that integrates the optical sensing capabilities of FBG with the high-temperature stability and selective adsorption properties of inorganic porous materials

Inventive Principle:
Principle #40Composite materials

2Measurement precision

If Pd coatings are used to detect hydrogen concentrations, then hydrogen detection is achieved, but the response time is quite long leading to hysteresis effects

Engineering Contradiction:
Improvehydrogen concentration detectionVSAvoidresponse time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent employs nanoporous materials with controlled pore sizes and high surface area-to-volume ratios, which enable rapid analyte diffusion and adsorption/desorption kinetics, significantly reducing response time and eliminating hysteresis effects while maintaining detection precision

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent creates localized sensing zones with specific nanoporous structures optimized for particular analytes, allowing different regions of the coating to have different pore sizes and chemical compositions tailored for fast response to specific gases

Inventive Principle:
Principle #3Local quality

3Measurement precision

If uniform FBG gratings are coated with sensor material, then the grating can detect axial strain, but the coating may cause temperature changes that affect measurement accuracy

Engineering Contradiction:
Improveaxial strain detection accuracyVSAvoidtemperature stability during measurement
Core Design Contradiction:
Measurement precisionVSTemperature

Solution Approach 1:

The patent replaces catalytic chemical reactions (which generate heat) with physical adsorption mechanisms in nanoporous materials, eliminating exothermic/endothermic effects that cause temperature fluctuations and measurement drift while maintaining strain detection capability

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The nanoporous coating structure inherently provides thermal stability and prevents temperature changes during measurement, making additional temperature compensation mechanisms unnecessary

Inventive Principle:
Principle #25Self-service

4Measurement precision

If catalytic materials are used in the sensor system, then gas detection sensitivity is improved, but the catalyst decomposition or poisoning limits the sensor lifetime

Engineering Contradiction:
Improvegas detection sensitivityVSAvoidsensor lifetime
Core Design Contradiction:
Measurement precisionVSDuration of action of stationary object

Solution Approach 1:

The patent replaces expensive, short-lived catalytic materials with stable, reusable inorganic nanoporous materials that can operate for extended periods without degradation, effectively creating a durable long-term sensing solution

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent converts the harmful effects of catalytic decomposition and poisoning into beneficial physical adsorption processes that are reversible and non-destructive, allowing the sensor to maintain sensitivity over long operational periods

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables continuous, reversible measurement of analytes like alkanes and alkanols with improved selectivity, accuracy, and robustness, suitable for extreme conditions, maintaining performance over long periods without degradation.

Implementation Method 1

The coating is capable of adsorption of the chemical substance of interest, whereby the coating swells or shrinks, which change is detectible by the optical detection unit

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

FBG act as selective mirrors in wavelength, reflecting some wavelengths around the Bragg wavelength, which equals two times the effective refractive index of the waveguide times the periodicity of the refractive index modulation

Methodology Applied
Scientific EffectBragg Diffraction: Bragg Diffraction

Data Source

PatentEP3149432B1A fiber bragg grating optical sensor having a nanoporous coating
Publication Date: 2019.02.20 NEDERLANDSE ORG VOOR TOEGEPAST NATUURWETENSCHAPPELIJK ONDERZOEK TNO
  • EP3149432B1 patent drawingFigure 1
  • EP3149432B1 patent drawingFigure 2~3
  • EP3149432B1 patent drawingFigure 4~5

AI summary

The invention relates to an optical waveguide having a Fibre Bragg Grating, which waveguide is provided with a coating comprising a nanoporous sensor material, the sensor unit further comprising an optical detection unit for detecting a change in an optical property of the waveguide, wherein the grating is present in the core of the waveguide, the coating at least substantially surrounds the grating, which coating is expandable or shrinkable under the influence of the chemical substance, thereby causing a change in axial strain in the grating when he sensor material is exposed to the chemical substance, which change is detectible by a optical detection unit. The invention further relates to an optical sensor system for measuring a chemical substance, the sensor system comprising a waveguide according to the invention.