Nano-Scale Diffusion Bonding for Dissimilar Material Seals

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Solution Overview

Problem

Traditional methods for bonding dissimilar materials like sapphire and titanium, such as diffusion bonding and soldering, often result in weak bonds, contamination, and damage to internal components due to high temperatures and pressures, and are prone to crack generation from thermal expansion mismatches.

Innovation Solution

A kinetically limited nano-scale diffusion bond is formed using an electromagnetic beam to bond transparent and absorbent materials at room temperature, creating a thin, crack-free, and hermetic interface with properties similar to the bulk materials, minimizing thermal stress and undesirable compound formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If traditional diffusion bonding is used to bond dissimilar materials, then bond strength is achieved, but high temperatures cause grain growth, alter physical properties, and generate cracks due to thermal expansion mismatch

Engineering Contradiction:
Improvebond strengthVSAvoidthermal damage and crack generation
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The invention changes the bonding parameters from high temperature (600-1000°C) to low temperature (room temperature or slightly elevated), and from long duration to short duration (kinetically limited process). This resolves the contradiction by achieving bond strength without the harmful thermal effects that cause grain growth, property alteration, and crack generation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the thermal field (heat-based diffusion bonding) with an electromagnetic field (laser or electron beam irradiation). This substitution enables bonding at low temperatures by using electromagnetic energy to drive the diffusion process locally at the interface, avoiding bulk heating and associated thermal damage.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Strength

If high temperature diffusion bonding is used, then material bonding is achieved, but internal components within the package are damaged by high temperatures

Engineering Contradiction:
Improvebond formationVSAvoiddamage to internal components
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The invention changes the temperature parameter from high (600-1000°C) to low (room temperature or slightly elevated), enabling bond formation without exposing internal components to damaging high temperatures. The kinetically limited process achieves bonding through short-duration electromagnetic irradiation rather than prolonged thermal exposure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention substitutes thermal energy with electromagnetic energy (laser or electron beam) to achieve bonding. This allows the bonding process to occur at low bulk temperatures, protecting temperature-sensitive internal components while still providing sufficient energy at the bond interface to create strong joints.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Area of stationary object

If traditional diffusion bonding creates large interaction zones, then bond coverage is achieved, but crack sizes increase and reliability decreases

Engineering Contradiction:
Improvebonded interface areaVSAvoidreliability and service life
Core Design Contradiction:
Area of stationary objectVSReliability

Solution Approach 1:

The invention creates a localized bond interface with distinct properties: a thin diffusion zone (nanometer to sub-micrometer scale) with high atomic mixing and a sharp transition to undisturbed bulk materials. This local quality approach concentrates the bonding action at the interface while preserving the integrity of the bulk materials, thereby achieving adequate bond area without the crack propagation issues associated with large interaction zones.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention changes the spatial scale parameter of the interaction zone from micrometer/millimeter scale (traditional diffusion bonding) to nanometer/sub-micrometer scale (kinetically limited bonding). This dramatic reduction in interaction zone size, achieved through short-duration electromagnetic irradiation, prevents crack initiation and propagation while maintaining sufficient bond strength across the interface.

Inventive Principle:
Principle #35Parameter changes

4Temperature

If intermediate layers like solder or glass frit are used for low temperature bonding, then bonding of dissimilar materials is achieved, but bond strength is inferior and susceptibility to corrosion increases

Engineering Contradiction:
Improvebonding temperatureVSAvoidbond strength and corrosion resistance
Core Design Contradiction:
TemperatureVSStrength

Solution Approach 1:

The invention extracts and eliminates the intermediate layer (solder, glass frit, or other bonding materials) from the bonding system. By using electromagnetic irradiation to directly induce diffusion bonding between the dissimilar materials at low temperatures, the process achieves strong, corrosion-resistant bonds without requiring separate bonding materials that would compromise strength or introduce corrosion vulnerabilities.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention uses electromagnetic radiation (laser or electron beam) as an intermediary energy source to enable direct bonding between dissimilar materials at low temperatures. This intermediary provides the necessary energy to drive diffusion at the interface without requiring thermal heating or intermediate bonding materials, thereby achieving both low temperature processing and superior bond strength with corrosion resistance.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces bonds with strength equivalent to the bulk materials, providing a hermetic, corrosion-resistant, and bio-stable connection without damaging the components, and is applicable to materials with varying thermal expansion coefficients.

Implementation Method 1

The absorbent opaque material has properties that significantly absorb energy from the electromagnetic beam

Methodology Applied
Scientific EffectElectromagnetic radiation absorption: Absorption (EM radiation)

Implementation Method 2

A kinetically limited nano-scale diffusion bond is formed using an electromagnetic beam to bond transparent and absorbent materials

Methodology Applied
Scientific EffectDiffusion bonding: Diffusion Welding

Data Source

PatentUS10981355B2Kinetically limited nano-scale diffusion bond structures and methods
Publication Date: 2021.04.20 MEDTRONIC INC
  • US10981355B2 patent drawing
  • US10981355B2 patent drawing
  • US10981355B2 patent drawing

AI summary

Bulk materials having a kinetically limited nano-scale diffusion bond is provided. The bulk materials having a kinetically limited nano-scale diffusion bond includes transparent material, absorbent opaque material and a diffusion bond. The transparent material has properties that allow an electromagnetic beam of a select wavelength to pass there through without more than minimal energy absorption. The absorbent opaque material has properties that significantly absorb energy from the electromagnetic beam. The diffusion bond is formed by the electromagnetic beam bonding the transparent material to the absorbent opaque material. Moreover, the diffusion bond has a thickness that is less than 1000 nm.