Nanostructured TCO Electrochromic Device Plasmon Resonance

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Solution Overview

Problem

Existing electrochromic technologies face challenges in stability under repeated cycling, limiting their application in smart window coatings, particularly due to the inability to dynamically modify the plasmon resonance frequencies of semiconductor nanocrystals and the formation of insulating barriers between nanostructures.

Innovation Solution

The development of an electrochromic device using nanostructured transparent conducting oxide (TCO) films, where the surface plasmon resonance is dynamically modulated through electrochemical doping, allowing for reversible changes in the free carrier concentration and dielectric environment, thereby enhancing the stability and optical properties of the films.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If semiconductor nanocrystals are used for electrochromic devices, then plasmon resonance frequency modulation is achieved, but stability under repeated cycling deteriorates due to insulating barrier formation

Engineering Contradiction:
Improveplasmon resonance frequency modulationVSAvoidstability under repeated cycling
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The patent changes the material parameter from semiconductor nanocrystals to transparent conducting oxide nanocrystals, which maintain high electrical conductivity after electrochemical doping. This parameter change eliminates the formation of insulating barriers while preserving the ability to modulate plasmon resonance frequency through electrochemical doping, thus resolving the contradiction between adaptability and reliability.

Inventive Principle:
Principle #35Parameter changes

2Stability of the object's composition

If hydrocarbon ligands are used to cap nanocrystal surfaces, then nanocrystal stability is improved, but electrical conductivity deteriorates due to insulating barriers between nanocrystals

Engineering Contradiction:
Improvenanocrystal surface stabilityVSAvoidelectrical conductivity
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent changes the ligand parameter from hydrocarbon ligands to short-chain carboxylic acid ligands. This parameter change reduces the insulating barrier thickness between nanocrystals, allowing electrical conductivity to be maintained or enhanced while preserving nanocrystal surface stability. The shorter ligand chain length enables better electrical coupling between adjacent nanocrystals.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses short-chain carboxylic acid ligands that can be easily exchanged or removed during processing. These short-living ligands serve their purpose of stabilizing nanocrystals during synthesis but are subsequently replaced or eliminated to achieve high conductivity in the final device, sacrificing the ligand's long-term stability function for the benefit of electrical conductivity.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves significant modulation of the plasmon resonance frequency, resulting in a high contrast ratio for near-infrared transmittance and improved durability, with minimal impact on visible light transmission, enabling robust and dynamic smart window performance.

Implementation Method 1

Localized surface plasmon absorption features arise at high doping levels in semiconductor nanocrystals, appearing in the near infrared range

Methodology Applied
Scientific EffectSurface plasmon resonance:

Implementation Method 2

the surface plasmon resonance is dynamically modulated through electrochemical doping, allowing for reversible changes in the free carrier concentration and dielectric environment

Methodology Applied
Scientific EffectElectrochemical doping:

Implementation Method 3

an electrochromic device using nanostructured transparent conducting oxide (TCO) films, where the surface plasmon resonance is dynamically modulated through electrochemical doping

Methodology Applied
Scientific EffectElectrochromism: Electrochromism

Data Source

PatentEP2748867B1Nanostructured transparent conducting oxide electrochromic device
Publication Date: 2019.03.13 RGT UNIV OF CALIFORNIA
  • EP2748867B1 patent drawingFigure 1
  • EP2748867B1 patent drawingFigure 2A
  • EP2748867B1 patent drawingFigure 2B

AI summary

The embodiments described herein provide an electrochromic device. In an exemplary embodiment, the electrochromic device includes (1) a substrate and (2) a film supported by the substrate, where the film includes transparent conducting oxide (TCO) nanostructures. In a further embodiment, the electrochromic device further includes (a) an electrolyte, where the nanostructures are embedded in the electrolyte, resulting in an electrolyte, nanostructure mixture positioned above the substrate and (b) a counter electrode positioned above the mixture. In a further embodiment, the electrochromic device further includes a conductive coating deposited on the substrate between the substrate and the mixture. In a further embodiment, the electrochromic device further includes a second substrate positioned above the mixture.