NdFeB Magnet Sintering Reducing Heavy Rare Earth
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Solution Overview
Problem
The increasing demand for NdFeB rare earth permanent magnetic materials in applications such as electronic components, energy-saving control motors, and wind power generation has led to a severe shortage of rare earth resources, particularly heavy rare earth elements, necessitating a method to reduce their usage while improving magnetic performance.
Innovation Solution
A continuous vacuum sintering method and apparatus are employed, involving a series of chambers for pre-heating, degassing, pre-sintering, sintering, aging, and cooling, with specific temperature and vacuum conditions to optimize the sintering process, and the use of micro powders like Dy2O3 to enhance the coercive force of the magnets.
Engineering Contradictions & Design Principles
Engineering Contradiction Analysis
1Strength
If heavy rare earth elements are added to improve coercive force, then magnetic performance is improved, but rare earth resource consumption increases
Solution Approach 1:
The patent applies local quality by concentrating heavy rare earth elements (Dy, Tb) specifically at the grain boundaries of the NdFeB magnet rather than uniformly distributing them throughout the material. This localized approach at the grain boundary phase achieves enhanced coercive force while minimizing overall rare earth consumption, directly resolving the technical contradiction between improving magnetic strength and reducing resource usage.
Solution Approach 2:
The patent employs parameter changes by precisely controlling the concentration and distribution of heavy rare earth elements in the grain boundary phase, optimizing their content to achieve maximum coercive force enhancement with minimum material usage. Additionally, the multi-stage sintering process parameters (temperature, time, atmosphere) are optimized to control grain growth and heavy rare earth distribution, further reducing rare earth consumption while maintaining high magnetic performance.
2Strength
If multi-stage sintering process is used to optimize magnetic performance, then coercive force is improved, but processing time and energy consumption increase
Solution Approach 1:
The patent applies segmentation by dividing the sintering process into multiple distinct stages: initial sintering stage (forming Nd2Fe14B phase and grain boundary phase), first aging stage (800-950°C for grain growth control), and second aging stage (different temperature for final optimization). Each stage serves a specific purpose in controlling microstructure evolution and heavy rare earth distribution, enabling optimized magnetic performance with controlled processing time.
Solution Approach 2:
The patent employs preliminary action by conducting the initial sintering stage to establish the basic microstructure and grain boundary phase formation before subsequent aging treatments. The first aging stage preliminarily controls grain growth and heavy rare earth distribution, preparing the microstructure for final optimization in the second aging stage. This sequential preliminary actions approach enables systematic microstructure control while managing overall processing time efficiently.
Applied Scientific Principles
This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.
Function Achieved in This Case
This approach results in high-performance NdFeB rare earth permanent magnets with improved coercive force and reduced rare earth usage, addressing the resource shortage and enhancing magnetic properties.
Implementation Method 1
pre-heating to remove organic impurities, and further for heating to dehydrogenate and degas
Implementation Method 2
continuous vacuum sintering furnace
Implementation Method 3
pre-sintering, sintering, aging and cooling
Implementation Method 4
rapidly cooling by gas
Data Source
AI summary
A method for sintering NdFeB rare earth permanent magnet includes steps of: providing a continuous vacuum sintering furnace to sinter; loading a sintering box with compacted magnet blocks onto a loading frame; while driving by a transmission apparatus, sending the loading frame orderly through a preparation chamber, a pre-heating and degreasing chamber, a first degassing chamber, a second degassing chamber, a pre-sintering chamber, a sintering chamber, an aging chamber and a cooling chamber of the continuous vacuum sintering furnace, respectively for pre-heating to remove organic impurities, and further for heating to dehydrogenate and degas, pre-sintering, sintering, aging and cooling. A continuous vacuum sintering apparatus is also provided.


