Nested Graphite Condensing Casings for Vacuum Refining

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Solution Overview

Problem

Conventional vacuum refining furnaces face issues with high temperature graphite condensing casings leading to decreased condensing efficiency, especially for metals with low boiling points like antimony and arsenic, resulting in reduced service life and obstructed exhaust pipes.

Innovation Solution

The design incorporates a nested structure of graphite condensing casings with varying diameters and through holes, allowing for progressive temperature reduction and increased condensing area, along with a graphite insulating casing to control heat transfer and prevent excessive temperature, enabling efficient condensation of metals with different boiling points.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Power

If the graphite heater power is increased to improve treating capacity, then the power increases, but the temperature of the graphite condensing casing becomes too high and condensing efficiency decreases

Engineering Contradiction:
Improvegraphite heater powerVSAvoidcondensing efficiency
Core Design Contradiction:
PowerVSReliability

Solution Approach 1:

The single condensing casing is divided into multiple graphite condensing casings with different diameters arranged in sequence. Each casing condenses metal vapors at different temperature zones, creating a segmented temperature control system that allows high power heating while maintaining effective condensation for various metal elements.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention transitions from a single-dimensional condensing structure to a multi-dimensional nested structure where condensing casings of different diameters are arranged concentrically. This spatial arrangement creates progressive temperature gradients, allowing the system to handle both high-temperature and low-temperature condensation requirements simultaneously.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Power

If the graphite heater power is increased to improve treating capacity, then the power increases, but metal vapor spreads and condenses randomly, obstructing exhaust pipes

Engineering Contradiction:
Improvegraphite heater powerVSAvoidrandom condensation and exhaust pipe obstruction
Core Design Contradiction:
PowerVSObject-generated harmful factors

Solution Approach 1:

Different regions of the condensing system are designed with different diameters and temperatures to match the condensation requirements of specific metal elements. Low-boiling-point metals like antimony and arsenic are condensed in outer casings with lower temperatures, while high-boiling-point metals are condensed in inner casings, preventing random condensation and exhaust pipe obstruction.

Inventive Principle:
Principle #3Local quality

3Device complexity

If a single graphite condensing casing is used, then the structure is simple, but the total condensing area is insufficient and condensing efficiency decreases

Engineering Contradiction:
Improvecondensing casing structureVSAvoidtotal condensing area
Core Design Contradiction:
Device complexityVSArea of stationary object

Solution Approach 1:

Multiple graphite condensing casings with different diameters are nested concentrically within each other, similar to nested dolls. This configuration maximizes the total condensing surface area within a compact space, allowing each casing to contribute to the overall condensation process at its optimal temperature zone.

Inventive Principle:
Principle #7Nested doll (Nesting)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration enhances condensing efficiency, increases treating capacity, and extends the service life of the furnace by effectively condensing metals difficult to handle, such as antimony and arsenic, while maintaining high power and flow speed, resulting in improved alloy refining capabilities.

Implementation Method 1

the metal of low boiling point is transformed from a liquid state to a gas state by evaporation

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

condensed to the liquid state again on the graphite condensing casing

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

the heat quantity from the graphite heater and the evaporation laminate is obstructed, and the temperature of the graphite condensing casing is controlled to be not too high

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Data Source

PatentEP2770068B1Vacuum refining furnace for nonferrous metal multicomponent alloys
Publication Date: 2017.06.21 KUNMING DIBOO TECH
  • EP2770068B1 patent drawingFigure 1
  • EP2770068B1 patent drawingFigure 2
  • EP2770068B1 patent drawingFigure 3

AI summary

Disclosed is a high-power vacuum refining furnace which can be used for the purification of the multicomponent alloys. The evaporator coil laminates are covered by a refining furnace graphite insulation screen wherein a number of through-holes are cast. The graphite condensation jackets are of two or more different sizes with the minimum located in the outside of the graphite insulation screen and the bigger one located in the outside of the smaller one. Except the maximum condensation jacket, all the condensation jackets are equipped with a number of through-holes. The following advantages are present: 1) refining a variety of multicomponent alloys with low-cost vacuum distillation; 2) when the power of the graphite heater reaches 270 kw, the processing capability of certain alloys can be up to 25 metric tons per day; 3) less heat loss, high efficiency of evaporation and condensation; 4) long working life, low energy consumption, high metal direct yield, good, stable and reliable production environment.