Nickel-Based Cathode Coating for Battery Stability

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Solution Overview

Problem

Nickel-based lithium metal oxide positive active materials in rechargeable lithium batteries face deteriorated cell characteristics due to side-reactions with electrolyte solutions, leading to increased charge transfer resistance and reduced power output.

Innovation Solution

A positive active material is developed with a nickel-based lithium metal oxide having a layered crystal structure and a selective coating layer of lithium-metal oxide on the (003) crystalline plane, minimizing lattice mismatch and preventing charge transfer resistance increase, while maintaining lithium ion intercalation and deintercalation efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If a nickel-based lithium metal oxide is used as a positive active material to improve capacity characteristics, then the discharge capacity is improved, but the cell characteristics deteriorate due to side-reactions with the electrolyte solution

Engineering Contradiction:
Improvedischarge capacityVSAvoidcell characteristics
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

A coating layer comprising a lithium-metal oxide is formed on the surface of the nickel-based lithium metal oxide particles. This coating layer acts as an intermediary barrier between the nickel-based lithium metal oxide and the electrolyte solution, preventing direct contact and side-reactions while allowing lithium ion transport, thus improving cell characteristics without sacrificing discharge capacity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The positive active material is designed as a composite structure combining nickel-based lithium metal oxide core particles with a lithium-metal oxide coating layer. This composite material approach allows the inner core to provide high capacity characteristics while the outer coating provides stability and prevents harmful side-reactions with the electrolyte solution

Inventive Principle:
Principle #40Composite materials

2Reliability

If a coating layer is formed on the nickel-based lithium metal oxide to prevent side-reactions, then the cell characteristics are improved, but the charge transfer resistance increases

Engineering Contradiction:
Improvecell characteristicsVSAvoidcharge transfer resistance
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The coating layer is designed with specific local properties: it comprises a lithium-metal oxide with a crystal structure having a specific lattice parameter ratio (c/a between 2.05 and 2.15), which creates favorable local crystallographic orientation and lattice matching at the interface with the nickel-based lithium metal oxide. This local structural quality enables efficient charge transfer while maintaining the protective function against side-reactions

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The crystal structure parameters of the lithium-metal oxide coating layer are precisely controlled, specifically the lattice parameter ratio (c/a) between 2.05 and 2.15, and the content of the lithium-metal oxide is optimized at 0.1-5 mol% based on the total amount of lithium metal oxide. These parameter optimizations ensure the coating layer provides protection without significantly increasing charge transfer resistance

Inventive Principle:
Principle #35Parameter changes

3Stability of the object's composition

If the lattice mismatch ratio is reduced to improve epitaxial growth, then the coating layer stability is improved, but the manufacturing precision requirements increase

Engineering Contradiction:
Improvecoating layer stabilityVSAvoidlattice mismatch control
Core Design Contradiction:
Stability of the object's compositionVSManufacturing precision

Solution Approach 1:

The patent specifies a range for the lattice parameter ratio (c/a between 2.05 and 2.15) and the lithium-metal oxide content (0.1-5 mol%) that optimizes lattice matching between the coating layer and the nickel-based lithium metal oxide. By controlling these parameters within specified ranges rather than requiring exact values, the patent achieves good epitaxial growth and coating stability while maintaining practical manufacturing feasibility

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enhances power output characteristics, improves electrode stability, and reduces gas generation at high voltages, ensuring improved reliability and safety of rechargeable lithium batteries.

Implementation Method 1

the lithium-metal oxide selectively disposed on the (003) crystalline plane of the nickel-based lithium metal oxide and the nickel-based lithium metal oxide may have a layered structure that is epitaxially grown in the same c-axis direction

Methodology Applied
Scientific EffectEpitaxial growth: Epitaxy

Implementation Method 2

A lattice mismatch ratio between a (003) plane of the nickel-based lithium metal oxide and a (001) plane (I is 1, 2, or 3) of the lithium-metal oxide may be less than or equal to about 15%

Methodology Applied
Scientific EffectLattice mismatch:

Implementation Method 3

a positive active material that easily intercalates/deintercalates lithium ions

Methodology Applied
Scientific EffectIntercalation:

Implementation Method 4

lithium ion intercalation and deintercalation efficiency

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP3733610A1Positive active material for rechargeable lithium battery, method of preparing the same, and rechargeable lithium battery including the same
Publication Date: 2020.11.04 SAMSUNG SDI CO LTD
  • EP3733610A1 patent drawingFigure 1
  • EP3733610A1 patent drawingFigure 2
  • EP3733610A1 patent drawingFigure 3A

AI summary

Disclosed are a positive active material for a rechargeable lithium battery including a nickel-based lithium metal oxide having a layered crystal structure and a coating layer including a lithium-metal oxide selevtively disposed on (003) crystalline plane of the nickel-based lithium metal oxide, wherein the positive active material includes at least one secondary particle including an agglomerate of two or more primary particles, a method of preparing the same, and a rechargeable lithium battery including the positive active material.