Nickel-Doped Ozone Electrode for Neutral Water Electrolysis

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Solution Overview

Problem

Existing methods for ozone generation in water face challenges in dissolving ozone in a gas phase and adjusting concentration, particularly in neutral aqueous solutions like city water, and there is a need for an electrode that can stably produce ozone with high efficiency and durability.

Innovation Solution

A catalyst layer composed of 79.0 mol % to 90.0 mol % tin oxide, 7.0 mol % to 17.0 mol % antimony oxide, and 0.1 mol % to 6.0 mol % nickel oxide is formed on a titanium or titanium alloy substrate, with a specific production method involving solution mixing, application, and heat treatment to create an electrode with high ozone generation efficiency and durability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a platinum wire electrode is used in acidic aqueous solution for ozone generation, then ozone can be generated by electrolysis, but the method requires sulfuric acid electrolyte which is difficult to handle and not suitable for neutral water like city water

Engineering Contradiction:
Improveozone generation stabilityVSAvoidelectrolyte handling ease
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The invention changes the chemical composition parameters of the catalyst layer by incorporating nickel oxide (0.1-6.0 mol%) alongside tin oxide and antimony oxide, which modifies the electrode's catalytic properties to enable effective ozone generation in neutral pH conditions without requiring acidic electrolytes

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses a composite catalyst layer material consisting of tin oxide, antimony oxide, and nickel oxide in specific ratios, combining the properties of these materials to achieve both high ozone generation efficiency and compatibility with neutral aqueous solutions like city water

Inventive Principle:
Principle #40Composite materials

2Productivity

If silent discharge method is used to generate ozone, then ozone can be produced in gas phase, but the ozone is difficult to dissolve in water and concentration adjustment is difficult

Engineering Contradiction:
Improveozone production capabilityVSAvoidconcentration adjustment ease
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The invention replaces the mechanical silent discharge method with an electrochemical electrolysis process using the specialized electrode, which directly generates ozone in aqueous solution through electron transfer reactions at the electrode surface, eliminating the need for gas dissolution and enabling precise concentration control through electrolysis parameters

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Productivity

If an electrode is designed for high ozone generation efficiency, then ozone production is enhanced, but the durability and stability in neutral aqueous solution may be compromised

Engineering Contradiction:
Improveozone generation efficiencyVSAvoidelectrode durability
Core Design Contradiction:
ProductivityVSDuration of action of stationary object

Solution Approach 1:

The invention employs a composite catalyst layer of tin oxide, antimony oxide, and nickel oxide where each material contributes specific properties: tin oxide provides catalytic activity, antimony oxide enhances stability, and nickel oxide improves durability in neutral conditions, achieving both high efficiency and long service life

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention applies the catalyst layer with specific compositional ratios (79-90 mol% tin oxide, 7-17 mol% antimony oxide, 0.1-6.0 mol% nickel oxide) to optimize local catalytic properties at the electrode surface, ensuring high ozone generation efficiency while maintaining overall structural durability

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The electrode achieves excellent ozone generation efficiency and durability in neutral aqueous solutions, with an electric double layer capacitance ranging from 2 (mC/cm2) to 40 (mC/cm2), enhancing catalyst utilization and stability.

Implementation Method 1

generating ozone through a reaction at an anode by the electrolysis of water

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Implementation Method 2

The above-mentioned electrode for ozone generation has a value of an electric double layer capacitance of from 2 (mC/cm2) to 40 (mC/cm2)

Methodology Applied
Scientific EffectElectric double layer capacitance: Capacitance

Data Source

PatentUS20250382715A1Electrode for ozone generation
Publication Date: 2025.12.18 ISHIFUKU METAL IND CO LTD

AI summary

An electrode for ozone generation has excellent ozone generation efficiency even in a neutral aqueous solution such as city water and has excellent durability. An electrode for electrolysis is specifically designed for ozone generation. The electrode for ozone generation includes an electrode substrate formed of titanium or a titanium alloy, and a catalyst layer formed on the electrode substrate, the catalyst layer consisting of 79.0 mol % or more and 90.0 mol % or less of tin oxide, 7.0 mol % or more and 17.0 mol % or less of antimony oxide, and 0.1 mol % or more than 0.1 mol % and 6.0 mol % or less of nickel oxide on a metal basis.