Thermocompensated Hairspring via Niobium Alloy Oxidation

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Solution Overview

Problem

Existing methods for manufacturing thermocompensated balance springs are costly and lack sufficient information on deformation and heat treatment steps required to achieve the desired crystallographic structure and properties.

Innovation Solution

A method involving a Niobium-Titanium, Niobium-Zirconium, or Niobium-Hafnium alloy blade, where the process includes oxidation of the surface, shaping by strapping, and a fixing heat treatment, allowing for a spiral spring with a near-zero coefficient of thermal expansion (CTE) to be achieved.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If multiple deformation and heat treatment steps are performed to achieve desired crystallographic structure, then Young's Modulus Thermal Coefficient is improved to +/- 10 ppm/°C, but manufacturing complexity and cost increase significantly

Engineering Contradiction:
ImproveYoung's Modulus Thermal CoefficientVSAvoidmanufacturing process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The blade surface is oxidized before shaping and heat treatment operations. This preliminary oxidation creates a surface layer with specific thermal expansion characteristics that will compensate for temperature variations in the final product, eliminating the need for complex post-processing steps to achieve the desired thermal properties

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention changes the physical-chemical state of the blade surface through controlled oxidation, creating a surface layer with different thermal expansion properties than the base material. By controlling oxidation depth and conditions, the thermal expansion characteristics can be precisely tuned to achieve near-zero CTE in the final hairspring

Inventive Principle:
Principle #35Parameter changes

2Reliability

If multiple deformation and heat treatment steps are performed to achieve desired crystallographic structure, then thermocompensation properties are improved, but production time and cost increase

Engineering Contradiction:
Improvetemperature stabilityVSAvoidmanufacturing cycle time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The invention combines multiple functions into the oxidation step: it creates the thermocompensation surface layer, prepares the surface for subsequent shaping operations, and establishes the foundation for achieving the desired crystallographic structure. This merging of functions reduces the total number of discrete manufacturing steps required

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

By performing oxidation before shaping and heat treatment, the invention establishes the thermal compensation characteristics early in the manufacturing process. Subsequent operations work with this pre-established surface layer, eliminating the need for additional specialized treatment steps that would otherwise be required to achieve temperature stability

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If oxidation is performed after shaping, then surface treatment is complete, but thermocompensation cannot be optimized

Engineering Contradiction:
ImproveCTE controlVSAvoidprocess simplicity
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The blade is oxidized while still in its blank state, before any shaping operations. This allows the oxidation process to penetrate and treat the entire surface area uniformly, and ensures that subsequent shaping operations deform the oxidized layer along with the base material, integrating the thermocompensation properties into the final geometry

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The oxidation creates a surface layer with locally different properties (different thermal expansion characteristics) compared to the bulk material. By controlling the oxidation depth, a gradient structure is created where the surface layer provides thermocompensation while the bulk material provides structural integrity

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method allows for the easy implementation of conventional tools and devices, achieving a spiral spring with a CTE close to zero, which can be varied by modifying the oxidation rate, thus effectively compensating for temperature variations.

Implementation Method 1

carrying out an oxidation of the surface of said blade to a predetermined depth for example by thermal oxidation

Methodology Applied
Scientific EffectThermal oxidation: Oxidation

Implementation Method 2

step d) is carried out by thermal oxidation, by heating said blade under the following conditions: temperature between 350°C and 700°C

Methodology Applied
Scientific EffectThermal heating: Heating

Implementation Method 3

carrying out a fixing heat treatment in order to freeze the shape of said blade that it has taken during the stripping

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Data Source

PatentEP4019459B1Method for manufacturing a thermocompensated hairspring
Publication Date: 2025.06.11 ATOKALPA SUCCURSALE DE ALLE DE SFF COMPOSANTS HORLOGERS SA
  • EP4019459B1 patent drawingFigure 1a~1c
  • EP4019459B1 patent drawingFigure 2
  • EP4019459B1 patent drawingFigure 3~4

AI summary

Method for manufacturing a spiral spring (1) for a balance-spring oscillator, comprising the steps of: a) obtaining a blade (3) of Niobium-Titanium, Niobium-Zirconium or Niobium-Hafnium alloy having a predetermined height (H) and thickness (E); b) carrying out a slapping of said blade to put said blade into the shape of a spiral; c) carrying out a fixing heat treatment to fix the shape of said blade (3); d) carrying out an oxidation of the surface of said blade (3) to a predetermined depth (P).