Niobium-Titanium Oxide Anode Particles for Fast-Charge Energy Density

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Solution Overview

Problem

Secondary batteries with carbon-based negative electrodes face issues such as dendrite precipitation, heat generation, and fires due to internal short circuits during rapid charge-and-discharge, while titanium oxide-based batteries have lower energy density and capacity due to their noble potential and limited lithium insertion sites.

Innovation Solution

An active material comprising niobium-containing oxide particles with protruded and recessed parts, specifically niobium-titanium composite oxides like Nb2TiO7, is used to enhance electrode performance, allowing for stable rapid charge-and-discharge and increased energy density by optimizing the shape and distribution of particles to improve electrolyte retention and lithium ion diffusion.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If titanium oxide is used as negative electrode material to enable rapid charge-and-discharge, then charge-and-discharge performance is improved, but energy density decreases due to higher potential and lower capacity per weight

Engineering Contradiction:
Improvecharge-and-discharge performanceVSAvoidenergy density
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent uses a composite oxide material containing both titanium and niobium elements (such as Nb2TiO7, Li2Nb2TiO7, or LiNb2TiO7) to combine the advantages of both materials. The titanium component provides rapid charge-and-discharge capability, while the niobium component increases capacity per weight, achieving both high productivity and high energy density simultaneously

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent modifies the chemical composition parameters by controlling the molar ratios of titanium to niobium (specifically 1:2 to 1:4 ratios) and adjusting lithium content to create optimal composite structures that balance potential, capacity, and energy density for both rapid charge-and-discharge and high energy storage

Inventive Principle:
Principle #35Parameter changes

2Use of energy by moving object

If electrode density is increased to improve energy density, then energy density is improved, but input/output performance deteriorates causing shortened charge-and-discharge life

Engineering Contradiction:
Improveenergy densityVSAvoidinput/output performance
Core Design Contradiction:
Use of energy by moving objectVSProductivity

Solution Approach 1:

The patent creates particles with non-spherical shapes featuring protruded and recessed parts, where the recessed parts specifically serve to retain electrolyte locally. This local structural feature ensures that even at high electrode densities, the electrolyte is retained at critical particle surfaces, maintaining good input/output performance while achieving high energy density

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent utilizes particles with surface recesses that create porous-like structures for electrolyte retention. These recessed parts act as electrolyte reservoirs, ensuring continuous ion transport pathways are maintained even when particles are densely packed in the electrode, thus preserving input/output performance at high densities

Inventive Principle:
Principle #31Porous materials

3Quantity of substance

If carbon-based negative electrode is used to achieve high capacity, then capacity per weight is improved, but dendrite precipitation and safety issues occur during rapid charge-and-discharge

Engineering Contradiction:
Improvecapacity per weightVSAvoidsafety and stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent converts the harmful effect of lithium instability into a benefit by using composite oxide materials that provide stable lithium insertion/extraction sites. The niobium-titanium composite structure creates ordered pathways for lithium ions, transforming the chaotic lithium deposition that causes dendrites into controlled, reversible lithium insertion, maintaining safety while achieving rapid charge-and-discharge capability

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The niobium-containing oxide particles with tailored shapes and structures enable high energy density, excellent rapid charge-and-discharge performance, and extended battery life by facilitating uniform lithium ion diffusion and maintaining electrolyte retention, thus addressing the limitations of previous materials.

Implementation Method 1

lithium is easily stabilized in the structure, whereby the substantial capacity decreases

Methodology Applied
Scientific EffectLithium ion diffusion: Diffusion

Implementation Method 2

the recessed parts serve to retain the electrolyte

Methodology Applied
Scientific EffectElectrolyte retention: Absorption (physical)

Data Source

PatentEP4245724A1Active material, electrode, secondary battery, battery pack, and vehicle
Publication Date: 2023.09.20 KK TOSHIBA
  • EP4245724A1 patent drawingFigure 1
  • EP4245724A1 patent drawingFigure 2
  • EP4245724A1 patent drawingFigure 3~4

AI summary

In general, according to one approach, an active material including particles containing a niobium-containing oxide is provided. The particles containing the niobium-containing oxide contain single particles (394) (501, 503, or 505) having protruded parts and recessed parts (502, 504). Three or more of the recessed parts (502, 504) satisfy 0.1 ≤ a/L ≤ 0.5 (1). Where L is a length of a tangent line in contact with a first protruded part (501, 505) and a second protruded part (503), and a is a maximum length of a perpendicular line from the tangent line to a recessed part (502, 504) defined by the first protruded part (501, 505) and the second protruded part (503).