Dual-Pressure Nitric Acid Plant Tail Gas Split to Eliminate Air Compression

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Solution Overview

Problem

Existing nitric acid production plants face high energy consumption and equipment revamping challenges, particularly due to the need for air and NOx gas compressors, leading to bottlenecks and significant costs.

Innovation Solution

A dual pressure nitric acid production system that recirculates tail gas and uses oxygen-rich gas from a high-pressure water electrolyzer to supply oxygen to the ammonia converter and NOx gas compressor, eliminating the need for an air compressor and optimizing ammonia conversion.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If air compressor and NOx gas compressor are used in dual pressure nitric acid production, then ammonia conversion and nitric acid production are achieved, but power consumption increases and equipment complexity increases

Engineering Contradiction:
Improvenitric acid productionVSAvoidpower consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent merges the functions of air compression and NOx gas compression into a single dual-stage compressor system. The first stage compresses air to intermediate pressure for ammonia oxidation, and the second stage compresses the resulting NOx gases to final pressure for absorption, eliminating the need for separate compressors and reducing overall power consumption.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The dual-stage compressor serves multiple functions: it acts as both an air compressor for the ammonia converter and an NOx gas compressor for the absorption tower. This multi-functional design reduces equipment count and simplifies the overall system while maintaining dual pressure operation capabilities.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Productivity

If air compressor and NOx gas compressor are used in dual pressure nitric acid production, then ammonia conversion and nitric acid production are achieved, but device complexity increases

Engineering Contradiction:
Improvenitric acid productionVSAvoidequipment complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent merges the functions of air compression and NOx gas compression into a single dual-stage compressor system. The first stage compresses air to intermediate pressure for ammonia oxidation, and the second stage compresses the resulting NOx gases to final pressure for absorption, eliminating the need for separate compressors and reducing overall power consumption.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The dual-stage compressor serves multiple functions: it acts as both an air compressor for the ammonia converter and an NOx gas compressor for the absorption tower. This multi-functional design reduces equipment count and simplifies the overall system while maintaining dual pressure operation capabilities.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Reliability

If traditional dual pressure system with separate compressors is used, then ammonia oxidation and NOx absorption are achieved, but equipment revamping costs increase

Engineering Contradiction:
Improveammonia conversion efficiencyVSAvoidequipment revamping costs
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent merges the functions of air compression and NOx gas compression into a single dual-stage compressor system. The first stage compresses air to intermediate pressure for ammonia oxidation, and the second stage compresses the resulting NOx gases to final pressure for absorption, eliminating the need for separate compressors and reducing overall power consumption.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The dual-stage compressor serves multiple functions: it acts as both an air compressor for the ammonia converter and an NOx gas compressor for the absorption tower. This multi-functional design reduces equipment count and simplifies the overall system while maintaining dual pressure operation capabilities.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Reduces power consumption, minimizes emissions, and simplifies the plant setup by removing the air compressor, while maintaining optimal ammonia conversion efficiency.

Implementation Method 1

ammonia is first oxidized in an ammonia burner on platinum gauzes (commonly called ammonia converter) or cobalt balls, producing nitric oxide

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

nitric oxide, following cooling, is then oxidized to nitrogen dioxide (NO2) and further to dinitrogen tetroxide N2O4 (g) in an oxidation section

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 3

cooling of nitrogen oxide gases is accomplished first through the use of a waste heat recovery system, then through the use of a cooler condenser in which condensed nitric acid is separated

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 4

By absorption in water, following compression through a NOx gas compressor, nitrogen dioxide and dinitrogen tetroxide are converted to nitric acid and nitric oxide

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Data Source

PatentEP4392368B1Dual pressure system for producing nitric acid and method of operating thereof
Publication Date: 2025.12.10 YARA INTERNATIONAL ASA
  • EP4392368B1 patent drawingFigure 1
  • EP4392368B1 patent drawingFigure 2A
  • EP4392368B1 patent drawingFigure 2B

AI summary

The present disclosure discloses a system for producing nitric acid at reduced power, the system being a standard dual pressure nitric acid plant characterised in that the system further comprises means for splitting a tail gas stream into a first tail gas stream, in fluid communication with an oxygen-rich gas upstream the ammonia mixing unit, and a second tail gas stream, and means for adjusting the amount of tail gas being split into the first tail gas stream and the second tail gas stream, such that an air compressor is not required for operating the nitric acid plant. The present disclosure further relates to a method for operating the system, to the use of the system of the disclosure for performing the method of the disclosure and to a method for revamping a standard dual pressure nitric acid plant into the system of the disclosure.