Nitride-Carbon Nanosheet Cathode Coating for Fast-Charge Stability

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Solution Overview

Problem

Existing coating methods for ternary positive electrode materials in lithium-ion batteries, such as gas phase deposition and one-step mixed sintering, are complex and prone to damaging the lattice structure of the material, affecting its performance.

Innovation Solution

A nitride/graphitized carbon nanosheet-coated ternary positive electrode material is developed, where the graphitized carbon is formed in situ during the nitride coating process, creating a denser conductive network and improving the material's rate performance and cycle stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If gas phase deposition coating method is used, then coating quality is improved, but process complexity increases and large-scale production becomes difficult

Engineering Contradiction:
Improvecoating qualityVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent replaces the complex gas phase deposition process with a simpler wet chemical coating method followed by low-temperature sintering. This substitution uses liquid precursors and chemical reactions instead of complex gas phase equipment and processes, achieving comparable or superior coating quality while dramatically simplifying the manufacturing process for large-scale production.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the processing parameters from high-temperature gas phase deposition to low-temperature wet chemical coating and sintering. By adjusting the coating temperature and using liquid precursors, the process becomes simpler and more suitable for large-scale production while maintaining coating quality.

Inventive Principle:
Principle #35Parameter changes

2Ease of manufacture

If one-step mixed sintering method is used, then process simplicity is improved, but lattice structure of ternary material is damaged

Engineering Contradiction:
Improveprocess simplicityVSAvoidlattice structure stability
Core Design Contradiction:
Ease of manufactureVSStability of the object's composition

Solution Approach 1:

The patent divides the coating process into separate steps: first coating the ternary material with a precursor solution, then performing low-temperature sintering to form the nitride coating. This segmentation allows the coating process to proceed at lower temperatures that do not damage the underlying ternary material lattice structure, while still achieving complete coating coverage.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent applies preliminary coating action by first depositing the nitride precursor on the ternary material surface, then performing low-temperature sintering to convert the precursor to nitride. This preliminary coating prevents direct exposure of the ternary material to harsh reducing gases, protecting the lattice structure while achieving effective coating.

Inventive Principle:
Principle #10Preliminary action

3Reliability

If oxide coating agent is used, then interface stability is improved, but electronic conductivity decreases

Engineering Contradiction:
Improveinterface stabilityVSAvoidelectronic conductivity
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The patent uses nitride compounds instead of oxide coating agents. Nitrides provide both the desired interface stability and superior electronic conductivity compared to oxides. The nitride coating forms a stable protective layer while maintaining good electrical conductivity, enabling fast ion conduction and meeting high current charging and discharging requirements.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed solution enhances the rate performance and cycle stability of the ternary positive electrode material, while simplifying the preparation method and making it suitable for large-scale industrial production.

Implementation Method 1

the coating element is coated on the surface of the ternary positive electrode material matrix by wet coating to obtain an intermediate product

Methodology Applied
Scientific EffectWet coating: Deposition (physical)

Implementation Method 2

the intermediate product is mixed with the carbonaceous and nitrogenous compound evenly, and the nitride/graphitized carbon nanosheet-coated ternary positive electrode material is obtained after sintering

Methodology Applied
Scientific EffectSintering: Sintering

Implementation Method 3

graphitized carbon is formed in situ in the coating process of the nitride

Methodology Applied
Scientific EffectGraphitization:

Implementation Method 4

The coating agent can also act as a fast ion conductor to provide a good channel for lithium ion diffusion and transmission

Methodology Applied
Scientific EffectIon conduction: Fast Ion Conductor

Data Source

PatentEP4322252B1Nitride/graphitized carbon nanosheet-coated ternary positive electrode material and preparation method therefor
Publication Date: 2025.05.14 GEM CO LTD

AI summary

The invention discloses a nitride/graphitized carbon nanosheet-coated ternary positive electrode material and preparation method therefor. The nitride/graphitized carbon nanosheet-coated ternary positive electrode material includes a ternary positive electrode material matrix and a coating layer; the coating layer is composed of nitride and graphitized carbon; and the graphitized carbon is formed in situ in the coating process of the nitride. Compared with a physical mixing method, the in-situ generated carbon layer is connected to the material matrix more tightly, and the formed conductive network is denser. So that the rate performance of the material is improved to the maximum extent. The preparation method is simple and easy to realize industrial production. And the obtained nitride/graphitized carbon nanosheet-coated ternary positive electrode material has excellent rate performance and cycling stability.