Nitrogen-Doped Carbon Coating for Solid-State Lithium Anodes

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Solution Overview

Problem

The growth of lithium dendrites during charging and discharging processes in all-solid-state batteries using lithium as an anode active material leads to short circuits and reduced battery capacity, posing significant challenges for commercialization.

Innovation Solution

An all-solid-state battery design incorporating a coating layer made of nitrogen-containing amorphous carbon, with specific nitrogen content and particle characteristics, is used to suppress lithium dendrite growth and improve charge/discharge characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If lithium is used as the anode active material to increase energy density, then the energy density of the all-solid-state battery is improved, but lithium dendrites grow through gaps in the solid electrolyte layer during charging and discharging, leading to short circuits or reduced battery capacity

Engineering Contradiction:
Improveenergy densityVSAvoidbattery stability
Core Design Contradiction:
Use of energy by moving objectVSReliability

Solution Approach 1:

A coating layer comprising amorphous carbon is introduced as an intermediary between the lithium anode active material and the solid electrolyte layer. This coating layer prevents direct contact and interaction between lithium and the solid electrolyte, thereby suppressing dendrite growth and eliminating short circuits while maintaining the high energy density benefits of lithium anode

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The coating layer is formed using composite materials including amorphous carbon, conductive polymer, and lithium salt, which combine the advantages of different materials to achieve both high conductivity and effective dendrite suppression, resolving the contradiction between energy density and reliability

Inventive Principle:
Principle #40Composite materials

2Reliability

If a coating layer comprising amorphous carbon is formed on the anode current collector to suppress lithium dendrite growth, then battery reliability is improved, but lithium diffusion resistance increases

Engineering Contradiction:
Improvedendrite suppressionVSAvoidlithium diffusion rate
Core Design Contradiction:
ReliabilityVSSpeed

Solution Approach 1:

The coating layer's physical and chemical parameters are optimized by controlling the amorphous carbon particle size (average 10-100 nm), nitrogen content (0.5-7 atomic%), and layer thickness (1-20 μm). These parameter adjustments reduce lithium diffusion resistance while maintaining effective dendrite suppression

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The coating layer is designed with non-uniform local properties, including nitrogen-doped regions for enhanced conductivity and specific particle size distributions, creating locally optimized zones that facilitate lithium diffusion while preventing dendrite formation in critical areas

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The battery exhibits excellent capacity retention and high-rate charging performance by minimizing lithium diffusion resistance and irreversible reactions, thereby enhancing battery stability and lifespan.

Implementation Method 1

the amorphous carbon comprises a nitrogen-containing amorphous carbon, and wherein a nitrogen amount (atomic %) included in the coating layer ranges from 0.5% to 7%

Methodology Applied
Scientific EffectNitrogen doping: Dopants

Implementation Method 2

90% or more of nitrogen in the nitrogen-containing amorphous carbon may be located within a depth of 5 nm from the surface of the nitrogen-containing amorphous carbon

Methodology Applied
Scientific EffectAdsorption: Adsorption

Data Source

PatentEP4651258A1All-solid-state battery, negative electrode assembly, and method for manufacturing same
Publication Date: 2025.11.19 LG ENERGY SOLUTION LTD
  • EP4651258A1 patent drawingFigure 1~2
  • EP4651258A1 patent drawingFigure 3~4
  • EP4651258A1 patent drawing

AI summary

The present invention relates to an all-solid-state battery comprising a positive electrode, a solid electrolyte layer, a coating layer, and a negative electrode current collector, wherein the coating layer comprises amorphous carbon, the amorphous carbon comprises nitrogen-containing amorphous carbon, and the nitrogen content (atomic %) contained in the coating layer is in the range of 0.5% to 7%. The all-solid-state battery according to the present invention may have an excellent capacity retention rate according to cycles during high-rate charging and discharging.