Nitrogen-Doped Carbon Catalyst Support for Fuel Cells

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Solution Overview

Problem

Existing catalyst support materials for polymer electrolyte fuel cells face challenges in achieving both high durability and efficient catalyst loading, often requiring high-temperature treatments that increase energy costs and risk noble metal catalyst aggregation.

Innovation Solution

A carbonized material is developed by carbonizing raw materials containing a nitrogen-containing organic substance and specific metals, resulting in a support with a unique graphite-like structure and amorphous component ratio, which enhances durability and catalyst loading efficiency without high-temperature treatments.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a highly crystalline carbon material such as graphite is used as catalyst support, then durability is improved, but the amount of catalyst that can be carried deteriorates due to small specific surface area

Engineering Contradiction:
ImprovedurabilityVSAvoidamount of catalyst
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The invention changes the structural parameters of carbon material by controlling the ratio of graphite-like structure (30-40%) to amorphous structure (60-70%), achieving an optimal balance between durability and surface area for catalyst support

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite carbon structure combining both graphite-like crystalline regions (providing durability) and amorphous regions (providing high surface area), rather than using purely crystalline or amorphous carbon

Inventive Principle:
Principle #40Composite materials

2Reliability

If high-temperature heating treatment is applied to increase graphitization, then durability is improved, but energy cost increases and noble metal catalyst aggregation occurs

Engineering Contradiction:
ImprovedurabilityVSAvoidenergy cost
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The invention incorporates metal elements during the carbonization process itself, before final structure formation, allowing the metal to influence carbon structure development at lower temperatures without requiring subsequent high-temperature graphitization treatments

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention achieves the desired carbon structure at lower temperatures by changing the chemical composition parameters (adding specific metals) rather than relying solely on thermal parameters (high-temperature treatment)

Inventive Principle:
Principle #35Parameter changes

3Reliability

If high-temperature heating treatment is applied to increase graphitization, then durability is improved, but noble metal catalyst aggregation occurs

Engineering Contradiction:
ImprovedurabilityVSAvoidcatalyst dispersion
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The metal elements are incorporated during carbonization to pre-form a stable distribution pattern that prevents catalyst aggregation, acting as a structural template before the final carbon structure develops

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The metal elements act as intermediaries that mediate between the carbonizing agents and the final carbon structure, controlling the formation process to achieve both durability and catalyst dispersion

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The support achieves high durability and catalyst performance, maintaining catalytic activity and reducing noble metal aggregation, while minimizing energy costs through a balanced graphite-like and amorphous structure, enabling efficient oxygen reduction activity.

Implementation Method 1

A carbonized material is developed by carbonizing raw materials containing a nitrogen-containing organic substance and specific metals

Methodology Applied
Scientific EffectCarbonization: Pyrolysis

Implementation Method 2

The PEFC is therefore expected to find applications in a power source for an electric vehicle... efficient oxygen reduction activity

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP2511008B1Support for catalyst supporting, material with supported catalyst, electrode, and cell
Publication Date: 2022.09.28 NISSHINBO HOLDINGS INC
  • EP2511008B1 patent drawingFigure 1
  • EP2511008B1 patent drawingFigure 2
  • EP2511008B1 patent drawingFigure 3(A)~4

AI summary

Provided is a support for carrying a catalyst capable of achieving both durability and ease of carrying a catalyst (performance of a catalyst support) at high levels. The support for carrying a catalyst is obtained by carbonizing raw materials containing a nitrogen-containing organic substance and a metal. The support for carrying a catalyst may have a peak at a diffraction angle of around 26° in an X-ray dif fraction pattern, the peak including 20 to 45% of a graphite-like structure component and 55 to 80% of an amorphous component. In addition, the support for carrying a catalyst may have an intensity ratio of a band at 1,360 cm-1 to a band at 1,580 cm-1 (I1,360/I1,580) in a Raman spectrum of 0.3 or more and 1.0 or less. In addition, the support for carrying a catalyst maybe obtained by carbonizing the raw materials to obtain a carbonized material, subjecting the carbonized material to a metal removal treatment, and subjecting the resultant to a heat treatment. In this case, the metal may be a transition metal.