NMR Spatial Permeability Profiling for Heterogeneous Rock Samples

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Solution Overview

Problem

Current probe permeameter techniques face limitations in measuring permeability of rock samples with rough surfaces, high pore connectivity, and heterogeneity, as they require a tight seal and are incapable of accurately measuring water permeability, especially in complex reservoir configurations.

Innovation Solution

The method employs nuclear magnetic resonance (NMR) to measure spatial water permeability by saturating and desaturating rock samples, performing T2 NMR measurements along multiple axes, and analyzing the data to derive spatial permeability profiles, which is non-destructive and not affected by the shape or composition of the rock sample.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If probe permeameter technique is used to measure permeability, then general heterogeneity of rock samples can be identified, but the technique fails to accurately measure water permeability in samples with rough surfaces, high pore connectivity, and heterogeneity

Engineering Contradiction:
Improvewater permeability measurement accuracyVSAvoidapplicability to heterogeneous rock samples
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent replaces the mechanical probe sealing system with a non-contact NMR measurement system. Instead of using a physical probe that requires tight sealing against the rock surface, the invention uses nuclear magnetic resonance to detect hydrogen signal intensities, eliminating the need for mechanical contact and sealing. This substitution enables accurate measurement of water permeability in heterogeneous samples with rough surfaces that would be difficult to seal properly.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the measurement parameter from direct pressure measurement (probe permeameter) to hydrogen signal intensity ratio (NMR). By measuring the ratio of hydrogen signal intensities in saturated and desaturated states, the system derives water permeability without requiring mechanical sealing. This parameter change allows the technique to work effectively on heterogeneous samples with varying pore structures and rough surfaces.

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If probe permeameter technique is used, then gas permeability can be measured, but the technique is incapable of accurately measuring water permeability

Engineering Contradiction:
Improvewater permeability measurement accuracyVSAvoidmeasurement reliability for different fluid types
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent uses hydrogen nuclei (protons) in water molecules as an intermediary to measure water permeability. The NMR technique detects the hydrogen signal intensity, which is directly related to the amount of water in the rock pores. By measuring the change in hydrogen signal intensity between saturated and desaturated states, the system reliably quantifies water permeability without being affected by the limitations of gas-based measurement methods.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Loss of information

If traditional permeability measurement techniques are used, then point measurements can be obtained, but continuous spatial permeability profile information cannot be derived

Engineering Contradiction:
Improvespatial permeability profile informationVSAvoidmeasurement system complexity
Core Design Contradiction:
Loss of informationVSDevice complexity

Solution Approach 1:

The patent transitions from point measurements to spatially distributed measurements by incorporating spatial encoding gradients in the NMR system. The measurement system acquires hydrogen signal intensities at multiple positions along the core sample axis, creating a continuous spatial profile of water permeability. This dimensional extension from single-point to multi-point measurement provides comprehensive spatial information without requiring complex arrays of physical probes.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach provides a robust and accurate method for determining spatial permeability profiles, overcoming the limitations of traditional techniques by offering precise measurements of water permeability in heterogeneous rock samples without damaging the samples.

Implementation Method 1

performing T2 NMR (nuclear magnetic resonance) on the saturated rock sample to detect spatial NMR data along a core sample axis

Methodology Applied
Scientific EffectNuclear magnetic resonance:

Implementation Method 2

detecting, with the NMR system, spatial NMR data along a core sample axis of the rock sample

Methodology Applied
Scientific EffectMagnetic field gradient: Magnetic Field

Data Source

PatentUS11821862B2Method for measuring the spatial water permeability profile of porous media by using non-destructive nuclear magnetic resonance technique
Publication Date: 2023.11.21 SAUDI ARABIAN OIL CO
  • US11821862B2 patent drawing
  • US11821862B2 patent drawing
  • US11821862B2 patent drawing

AI summary

A method includes deriving spatial permeability along a core axis by saturating the rock with an aqueous solution, performing T2 NMR on the saturated rock to detect spatial NMR data along the core axis, desaturating the rock, performing T2 NMR on the desaturated rock to detect spatial NMR data along the core axis, determining the spatial cutoff data for the saturated and desaturated rock along the core axis, and analyzing the spatial NMR data. The method further includes deriving spatial permeability along a second core axis by additionally performing T2 NMR on the saturated rock to detect spatial NMR data along a second core axis, performing T2 NMR on the desaturated rock to detect spatial NMR data along a second core axis, and determining the spatial cutoff data for the saturated and desaturated rock along the second core axis.