Liquid Nutritional Stabiliser System Preventing Phase Separation

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Solution Overview

Problem

Liquid nutritional compositions, particularly those containing partially hydrolysed protein and fat, face stability issues due to phase separation over time, exacerbated by ingredients like hydrolysed proteins and heat treatments, which can affect consumer perception despite not impacting nutritional quality.

Innovation Solution

A stabiliser system comprising a combination of emulsifiers with specific hydrophilic lipophilic balance values and low amylose starch, where hydrophobic and hydrophilic emulsifiers interact with low amylose starch to provide effective stability, including 0.1 to 10 grams/liter of each emulsifier and 0.01 to 20 grams/liter of low amylose starch.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If liquid nutritional compositions are stored for any length of time, then phase separation occurs and the product appears curdled, but the nutritional quality and efficacy remain unaffected

Engineering Contradiction:
Improveemulsion stabilityVSAvoidproduct acceptability
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

The patent applies composite materials by combining multiple stabilisers including high amylose starch, guar gum, and other hydrocolloids in specific proportions. This composite stabiliser system creates a synergistic effect that maintains emulsion stability and prevents phase separation better than individual stabilisers alone, thereby preserving product acceptability over storage time.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent employs parameter changes by adjusting the molecular weight, degree of substitution, and concentration of stabilisers to optimize emulsion stability. By modifying these parameters, the stabiliser system effectively prevents phase separation and maintains homogeneous appearance throughout the storage period.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If hydrolysed proteins and egg phospholipids are used in the composition, then nutritional quality is improved, but phase separation is exacerbated

Engineering Contradiction:
Improvenutritional contentVSAvoidemulsion stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent uses stabilisers such as high amylose starch and guar gum as intermediary substances that mediate between the hydrolysed proteins and fat phases. These stabilisers form a protective network that prevents direct interaction causing phase separation, thereby maintaining emulsion stability while preserving the nutritional benefits of hydrolysed proteins and egg phospholipids.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If heat treatments are applied to ensure sterility, then product safety is improved, but phase separation is worsened

Engineering Contradiction:
Improveproduct sterilityVSAvoidemulsion stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent applies beforehand cushioning by incorporating heat-stable stabilisers that pre-buffer the emulsion against the destabilizing effects of subsequent heat treatments. These stabilisers maintain their structural integrity during sterilization processes, preventing phase separation that would otherwise occur due to heat-induced changes in protein and fat phases.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The stabiliser system effectively prevents phase separation in liquid nutritional compositions, maintaining product quality and acceptability by ensuring a stable emulsion over time, as demonstrated by improved emulsion stability and re-dispersibility in examples.

Implementation Method 1

a stabiliser system comprising high amylose starch and guar gum

Methodology Applied
Scientific EffectEmulsion: Emulsion

Implementation Method 2

a combination of emulsifiers with a low amylose starch forms a particularly effective stabiliser system

Methodology Applied
Scientific EffectHydrophobic and hydrophilic interactions: Hydrophobe

Data Source

PatentUS8163320B2Stabiliser system for liquid nutritional compositions
Publication Date: 2012.04.24 SOCIETE DES PRODUITS NESTLE SA

AI summary

A liquid nutritional composition includes partially hydrolysed protein, fat and from 0.1 to 10 grams per liter of an emulsifier with a hydrophilic lipophilic balance value of less than 5, from 0.1 to 10 grams per liter of an emulsifier with a hydrophilic lipophilic balance value of more than 5 and from 0.01 to 20 grams per liter of a low amylose starch is shown.