Nylon Masterbatch Blending for Low-Heat Cable Jacketing Compounds

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Solution Overview

Problem

Traditional methods for producing nylon compounds for wire and cable jacketing involve high heat history and inefficient additive incorporation, limiting flexibility and uniformity in the final product.

Innovation Solution

A method involving the combination of a masterbatch with a high additive concentration and a resin with a low or no additive concentration, allowing for precise control of additive levels and reduced heat exposure, which includes incorporating additives into a polymer resin at a temperature above its melt point and pelletizing to create a more uniform mix.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If the entire formulation is compounded in a twin screw extruder to homogeneously incorporate additives, then uniformity of additive distribution is improved, but heat history of the nylon is increased

Engineering Contradiction:
Improveuniformity of additive distributionVSAvoidheat history
Core Design Contradiction:
Stability of the object's compositionVSTemperature

Solution Approach 1:

The compounding process is divided into two separate stages: first, additives are incorporated into a portion of the nylon resin to create a masterbatch compound; second, the masterbatch compound is blended with remaining nylon resin to achieve the final formulation. This segmentation allows each stage to be optimized independently, reducing overall heat exposure while maintaining uniform additive distribution.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The masterbatch compound is prepared in advance with concentrated additives, then stored and later blended with the base resin. This preliminary action separates the additive incorporation step from the final mixing step, allowing the majority of resin to avoid repeated heating cycles while still achieving homogeneous distribution through the blending operation.

Inventive Principle:
Principle #10Preliminary action

2Stability of the object's composition

If traditional compounding methods are used, then complete incorporation of all additives is achieved, but flexibility in selecting additive concentration levels is reduced

Engineering Contradiction:
Improvecomplete incorporation of additivesVSAvoidflexibility in selecting additive concentration levels
Core Design Contradiction:
Stability of the object's compositionVSAdaptability or versatility

Solution Approach 1:

The invention enables flexible control of additive concentration by varying the ratio of masterbatch compound to base resin in the final blend. By changing this mixing ratio parameter, different target concentrations can be achieved while maintaining complete incorporation of additives through the masterbatch preparation step.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The formulation is segmented into a concentrated masterbatch portion and a base resin portion. This segmentation allows the masterbatch to serve as a standardized additive source that can be mixed in varying proportions to achieve different final concentrations, providing versatility without compromising additive incorporation completeness.

Inventive Principle:
Principle #1Segmentation

3Stability of the object's composition

If all nylon resin is processed with additives in one step, then uniform compound is produced, but mixing capacity is reduced

Engineering Contradiction:
Improveuniformity of compoundVSAvoidmixing capacity
Core Design Contradiction:
Stability of the object's compositionVSProductivity

Solution Approach 1:

The nylon resin is divided into two functional portions: one portion is processed with additives to create the masterbatch compound, while the other portion remains as base resin for blending. This segmentation increases mixing capacity by allowing parallel processing of different resin portions and enabling the use of larger, more efficient mixers for the final blending operation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The masterbatch compound serves as an intermediary material that carries concentrated additives and facilitates their distribution throughout the final product. This intermediary approach improves mixing capacity by reducing the total amount of additive-containing material that requires intensive mixing, as the masterbatch acts as a pre-prepared intermediate that distributes additives efficiently during the final blending step.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces the heat history of the nylon, enhances mixing capacity, and allows for flexible selection of additive concentrations, resulting in improved properties such as tensile and flexural strength and modulus without significant differences between wholly compounded and masterbatch samples.

Implementation Method 1

incorporating the additives into the polymer resin at a temperature above the melt point of the polymer resin

Methodology Applied
Scientific EffectMelting: Melting

Data Source

PatentEP2864398B1Method and compositions for producing polymer blends
Publication Date: 2024.01.03 HONEYWELL INTERNATIONAL INC
  • EP2864398B1 patent drawingFigure 1
  • EP2864398B1 patent drawingFigure 2
  • EP2864398B1 patent drawingFigure 3

AI summary

Methods for mixing nylon compounds and compositions useful in mixing nylon compounds are provided. The methods and compositions disclosed are useful in producing nylon for wire and cable jacketing. The disclosed methods provide nylon having a reduced heat history compared to traditional methods. The disclosed methods and composition provide additional mixing capacity by reducing the amount of nylon that must be incorporated with additives per unit of final nylon composition. The disclosed methods and compositions provide the ability to select from a plurality of additive concentration levels in the final product by varying the ratio of a masterbatch compound containing a high concentration of the additive to a resin containing a low concentration or no additive.