Adjustable Mask Curtains for OES Signal Optimization

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Solution Overview

Problem

Conventional optical emission spectroscopic instruments face challenges in achieving optimal signal-to-noise ratios due to fixed mask configurations, which are not tailored to specific sample types, leading to suboptimal analysis and labor-intensive adjustments.

Innovation Solution

An adjustable mask system controlled by a processor that dynamically adjusts the field of view by opening or closing curtains to optimize the mask opening size and position based on real-time signal analysis, ensuring maximum signal and minimal noise levels.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a fixed mask configuration is used, then the instrument structure is simple, but the signal-to-noise ratio is suboptimal and analysis accuracy is compromised

Engineering Contradiction:
Improvesignal-to-noise ratioVSAvoidmask configuration complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The mask transitions from a fixed configuration to a dynamic, adjustable system with movable curtains that can be repositioned based on real-time signal analysis. The processor controls the mask position and opening size to optimize the field of view for different sample types, thereby improving signal-to-noise ratios while adapting to varying analytical requirements.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The system changes mask parameters including position, opening size, and curtain configuration based on real-time signal characteristics. The processor analyzes optical signals and adjusts mask parameters accordingly to maximize signal quality and minimize noise for different sample types and analytical conditions.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If a fixed mask configuration is used, then the instrument is easier to manufacture, but manual adjustments are labor-intensive and time-consuming

Engineering Contradiction:
Improveanalysis efficiencyVSAvoidmanual adjustment requirement
Core Design Contradiction:
ProductivityVSEase of operation

Solution Approach 1:

The system performs self-adjustment by automatically analyzing optical signals and modifying mask parameters without requiring manual intervention. The processor monitors signal characteristics and autonomously optimizes the mask configuration, eliminating labor-intensive manual adjustments and improving productivity.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The system implements a feedback loop where the processor continuously monitors optical signals from the sample analysis and uses this information to adjust mask parameters in real-time. This closed-loop control ensures optimal performance automatically, reducing the need for manual tuning and increasing analysis efficiency.

Inventive Principle:
Principle #23Feedback

3Adaptability or versatility

If a fixed mask configuration is used, then the instrument has stable performance, but it cannot be adapted to various sample types

Engineering Contradiction:
Improvesample type adaptabilityVSAvoidperformance stability
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The mask system becomes dynamic and adaptable to different sample types through automated adjustment. The processor modifies mask position and opening size based on real-time signal analysis, enabling the instrument to optimize performance for various samples while maintaining reliable and consistent analytical results through controlled, automated changes.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances signal-to-noise ratios, improves analysis accuracy, and reduces the need for manual adjustments, making the system more efficient and adaptable for various sample types.

Implementation Method 1

Optical emission spectroscopy (OES) is a mature, robust technology for the elemental analysis of materials. In OES, a small quantity of sample material is vaporized and excited above atomic ground state. Emissions characteristic of elements in the vaporized sample are captured by a light guide, which sends the light to a spectrometer, which produces and analyzes a spectrum from the light

Methodology Applied
Scientific EffectOptical emission spectroscopy: Absorption Spectroscopy

Implementation Method 2

For electrically conductive samples, prevalent techniques for generating emission spectra use either an electric arc or a spark, or both, to vaporize a small quantity of the sample to be analyzed. An electrical potential in an analytical gap between a counterelectrode and a surface of the sample breaks down gas in the gap, enabling an electrical current, in the form of a spark or an arc or both, to flow between counterelectrode and the sample surface

Methodology Applied
Scientific EffectElectric arc: Electric Arc

Implementation Method 3

An electrical potential in an analytical gap between a counterelectrode and a surface of the sample breaks down gas in the gap, enabling an electrical current, in the form of a spark or an arc or both, to flow between counterelectrode and the sample surface

Methodology Applied
Scientific EffectSpark: Electric Spark

Implementation Method 4

In the resulting plasma, the excited sample ('analyte') produces an optical (although possibly invisible) discharge that is characteristic of the elemental composition of the excited material

Methodology Applied
Scientific EffectPlasma: Plasma

Implementation Method 5

In the resulting plasma, the excited sample ('analyte') produces an optical (although possibly invisible) discharge that is characteristic of the elemental composition of the excited material

Methodology Applied
Scientific EffectOptical discharge: Electroluminescence

Implementation Method 6

A mask and/or a suitably short slit may be used to exclude these unwanted emissions

Methodology Applied
Scientific EffectOptical blocking: Absorption (EM radiation)

Implementation Method 7

Emissions characteristic of elements in the vaporized sample are captured by a light guide, which sends the light to a spectrometer

Methodology Applied
Scientific EffectLight transmission: Optical Fibre

Data Source

PatentUS9494463B2Optical emission spectroscopic (OES) instrument with automatic top and bottom slit curtains
Publication Date: 2016.11.15 THERMO SCIENTIFIC PORTABLE ANALYTICAL INSTRUMENTS INC
  • US9494463B2 patent drawing
  • US9494463B2 patent drawing
  • US9494463B2 patent drawing

AI summary

An optical emission spectroscopic (OES) instrument includes a spectrometer, a processor and an adjustable mask controlled by the processor. The adjustable mask defines a portion of an analytical gap imaged by the spectrometer. The instrument automatically adjusts the size and position of an opening in the mask, so the spectrometer images an optimal portion of plasma formed in the analytical gap, thereby improving signal and noise characteristics of the instrument, without requiring tedious and time-consuming manual adjustment of the mask during manufacture or use.