Off-Gas Analyzer with Heated Sampling Cell for Dusty Furnace Streams

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Solution Overview

Problem

Current off-gas analysis technologies, such as extractive and in situ laser systems, face limitations in analytical capabilities, precision, reliability, and maintenance costs, particularly in harsh industrial environments like steelmaking processes, where they struggle with particulate interference and require frequent recalibration and extensive maintenance.

Innovation Solution

A novel system that combines elements of extractive and in situ methods, using a compact, electronically linked off-gas analyzer with a fluid-cooled probe and tunable diode lasers to analyze dusty, high-temperature off-gases, allowing for uninterrupted full-spectrum analysis of H2O vapor, CO, O2, CO2, and H2 with reduced response times and minimal maintenance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If in situ laser systems transmit beams through off-gas in the fume duct, then off-gas chemistry analysis is achieved, but laser beam attenuation occurs due to particulate matter scattering and blocking

Engineering Contradiction:
Improveoff-gas chemistry analysis capabilityVSAvoidlaser beam transmission reliability
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent extracts the laser beam transmission path from the harsh off-gas environment by using an extractive sampling system. The laser beams are transmitted through a clean sample gas stream that has been separated from the dusty off-gas flow, eliminating particulate interference while maintaining analysis capability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a sample gas stream as an intermediary medium. This intermediary carries the off-gas components to the analysis chamber while providing a clean transmission path for laser beams, mediating between the harsh measurement environment and the sensitive optical detection system.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Adaptability or versatility

If extractive systems use vacuum pumps to extract and transport off-gas samples through heated conduits, then complete off-gas analysis spectrum is achieved, but analytical response delay increases due to sample transport time

Engineering Contradiction:
Improveoff-gas analysis spectrum coverageVSAvoidanalytical response delay
Core Design Contradiction:
Adaptability or versatilityVSLoss of time

Solution Approach 1:

The patent performs preliminary filtering of particulate matter from the off-gas sample before the gas enters the analysis chamber. This preliminary action ensures that the laser transmission path is clear from the start, eliminating delays caused by particulate interference and enabling immediate analysis.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent segments the analysis system into distinct functional zones: a sampling region where off-gas is extracted, a filtering region where particulates are removed, and an analysis region where laser transmission occurs. This segmentation allows each function to be optimized independently, maintaining fast response while achieving complete spectral analysis.

Inventive Principle:
Principle #1Segmentation

3Reliability

If in situ laser systems employ multiple purged probes extending into the fume duct to reduce path length, then laser beam attenuation is minimized, but device complexity and maintenance requirements increase

Engineering Contradiction:
Improvelaser beam transmission reliabilityVSAvoidprobe system complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent extracts only the necessary gas sample components into a separate analysis chamber, eliminating the need for complex in-duct probe arrangements. By taking the measurement out of the harsh environment rather than bringing the measurement equipment into the harsh environment, the system achieves reliability with simpler architecture.

Inventive Principle:
Principle #2Taking out (Extraction)

4Measurement precision

If conventional extractive systems require periodic recalibration with specialized calibration gases, then measurement precision is maintained, but maintenance costs and operational complexity increase

Engineering Contradiction:
Improveoff-gas analysis precisionVSAvoidsystem maintenance requirements
Core Design Contradiction:
Measurement precisionVSEase of repair

Solution Approach 1:

The patent implements a self-calibrating mechanism using reference gas channels that continuously monitor and adjust the laser transmission baseline. The system performs self-diagnosis and self-correction of drift conditions without requiring external calibration gases or manual intervention, maintaining precision while eliminating complex maintenance requirements.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves analytical response times of as short as 0.5 to 4 seconds and provides uninterrupted full-spectrum analysis, improving reliability and reducing maintenance costs by filtering particulate matter and eliminating the need for environmental enclosures and frequent calibration.

Implementation Method 1

a filter assembly for filtering particulate matter from the gas sample prior to analysis by the gas component measuring cell

Methodology Applied
Scientific EffectPhysical filtration: Filter (physical)

Implementation Method 2

an optical head being positioned towards the sampling chamber first ends, the optical head adapted for optical coupling to a coherent light source and including a plurality of emitters, said emitters being positioned to transmit a coherent light beam along a sampling chamber

Methodology Applied
Scientific EffectLight transmission: Light

Implementation Method 3

a detector assembly being positioned towards the sampling chamber second ends, the detector assembly provided for electronic coupling to a gas analyzer and including at least one detector for receiving said coherent light beams emitted from the emitters

Methodology Applied
Scientific EffectPhotoelectric detection: Photoelectric Effect

Implementation Method 4

a pump assembly operable to convey the off-gas samples from the gas sample source through the filter assembly and into the measuring cell for analysis

Methodology Applied
Scientific EffectMechanical pumping: Pump

Data Source

PatentEP3180598B1System and method for analyzing dusty industrial off-gas chemistry
Publication Date: 2024.03.06 TENOVA GOODFELLOW INC
  • EP3180598B1 patent drawingFigure 1
  • EP3180598B1 patent drawingFigure 1A
  • EP3180598B1 patent drawingFigure 1B

AI summary

An off-gas analyzer for analyzing H2O vapor, CO, O2, CO2 and/or H2 in a furnace gas stream is fluidically coupled to a gas extraction probe. The analyzer includes an optical measurement cell having multiple sampling chambers, optically coupled to a laser. The analyzer measuring cell is housed within a heated cabinet having a heater operable to heat the interior thereof so as to maintain the extracted gas sample therein at a temperature about the condensation point of water. The analyzer allows for the analysis of the gas water vapour of wet off-gas samples.