Olefin Polymerization Catalyst Using Non-Linear Alkyl Electron Donor

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Solution Overview

Problem

Existing catalysts for olefin polymerization, particularly those using dialkoxy magnesium carriers, face challenges in achieving wide molecular weight distribution, good stereospecificity, and processability while maintaining high polymerization activity and particle shape.

Innovation Solution

A solid catalyst component comprising a reaction product of a dialkoxy magnesium carrier, a titanium compound, and an internal electron donor, specifically a 2,3-di-non-linear-alkyl-2-cyano succinic acid diester or 2-isopropyl-2-(3-methylbutyl)-1,3-dimethoxy propane, in an inert solvent, which enhances polymer properties when used in olefin polymerization.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Shape

If a dialkoxy magnesium carrier is used to prepare a catalyst component for olefin polymerization, then good particle shape and stereosspecificity are obtained, but the molecular weight distribution is wide and processability is poor

Engineering Contradiction:
Improveparticle shapeVSAvoidprocessability
Core Design Contradiction:
ShapeVSEase of manufacture

Solution Approach 1:

The patent changes the chemical structure parameter of the internal electron donor from conventional phthalates to 2-isopropyl-2-(3-methylbutyl)-1,3-dimethoxypropane. This structural parameter change fundamentally alters the catalyst's polymerization behavior, enabling simultaneous achievement of good particle shape, narrow molecular weight distribution, and excellent processability by modifying how the electron donor interacts with the titanium center during polymerization

Inventive Principle:
Principle #35Parameter changes

2Productivity

If phthalate internal electron donors are used, then high polymerization activity and good stereosspecificity are achieved, but molecular weight distribution is wide and processability is poor

Engineering Contradiction:
Improvepolymerization activityVSAvoidprocessability
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The patent changes the chemical structure parameter of the internal electron donor from conventional phthalates to 2-isopropyl-2-(3-methylbutyl)-1,3-dimethoxypropane. This structural parameter change fundamentally alters the catalyst's polymerization behavior, enabling simultaneous achievement of good particle shape, narrow molecular weight distribution, and excellent processability by modifying how the electron donor interacts with the titanium center during polymerization

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If heating rate is controlled within 0.5-20°C/min to obtain solid catalyst component, then high isotacticity and bulk density are achieved, but fine powder content is high

Engineering Contradiction:
ImproveisotacticityVSAvoidfine powder content
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

The patent changes the chemical composition parameter by using 2-isopropyl-2-(3-methylbutyl)-1,3-dimethoxypropane as internal electron donor instead of conventional phthalates. This compositional change modifies the polymerization mechanism to produce polymers with better particle morphology and reduced fine powder content, while maintaining high isotacticity through the electron donor's stereospecific influence on the catalyst

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst achieves wide molecular weight distribution, good stereospecificity, and improved processability of the resulting polymers, with low fine powder content and high polymerization activity, making it suitable for applications requiring high processability.

Implementation Method 1

a solid catalyst component comprising a reaction product of a dialkoxy magnesium carrier, a titanium compound and an internal electron donor in an inert solvent

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentUS9376513B2Solid catalyst component and catalyst for olefin polymerization
Publication Date: 2016.06.28 CHINA PETROLEUM & CHEMICAL CORP

AI summary

Disclosed is a solid catalyst component for olefin polymerization. The catalyst component comprises a dialkoxy magnesium carrier, a titanium compound, and a product from an internal electron donor reacting in an inert solvent. The internal electron donor compound comprises a 2,3-di-non-linear-alkyl-2-cyano succinic acid diester compound as presented in formula I.