Oligo-Modified Nucleotide Adapters for Strand-Preserving Library Prep

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Solution Overview

Problem

Existing nucleic acid sequencing library preparation methods involve inefficient and loss-prone adapter addition processes, requiring additional purification steps and leading to sample loss due to incorrect adapter combinations and loss of strandedness information.

Innovation Solution

The use of oligo-modified nucleotide analogues with oligonucleotide adapters that are directly incorporated onto nucleic acids via polymerase-mediated reactions, allowing for efficient 3' adapterization and simplifying workflows, including asymmetric adapter addition without sample loss.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If ligation of adapters onto nucleic acid ends is used, then adapters can be added to nucleic acids, but sample loss occurs due to incorrect adapter combinations and additional purification steps are required

Engineering Contradiction:
Improveadapter addition processVSAvoidsample loss
Core Design Contradiction:
Ease of manufactureVSLoss of substance

Solution Approach 1:

The adapter is pre-coupled to a nucleotide analogue before the nucleotide is incorporated into the nucleic acid. This preliminary attachment ensures the adapter is already in position and correctly oriented when polymerase incorporates the modified nucleotide, eliminating the need for subsequent ligation steps and preventing sample loss from incorrect adapter combinations.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The mechanical/chemical ligation process is replaced by polymerase-mediated incorporation. Instead of using ligase to join adapters to nucleic acid ends, the polymerase incorporates the modified nucleotide (with pre-coupled adapter) into the growing nucleic acid chain, substituting a biochemical process for a chemical/mechanical one that is more precise and eliminates purification steps.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Productivity

If ligation reaction is used to add adapters, then adapters can be incorporated onto nucleic acids, but additional purification steps are necessary to remove undesired ligation products

Engineering Contradiction:
Improveadapter incorporation efficiencyVSAvoidpurification steps
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The adapter is pre-coupled to the nucleotide analogue in a controlled manner before incorporation. This ensures that when the polymerase incorporates the modified nucleotide, the adapter is already correctly positioned and oriented, producing only the desired product without undesired ligation products that would require purification.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The ligation reaction and subsequent purification steps are replaced by a single polymerase incorporation step. The polymerase reads the template and incorporates the modified nucleotide with the pre-coupled adapter, creating the final product in one biochemical step without generating byproducts that need removal.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Adaptability or versatility

If universal adapters are added using conventional methods, then sequencing libraries can be prepared, but strandedness information is lost

Engineering Contradiction:
Improveuniversal adapter compatibilityVSAvoidstrandedness information
Core Design Contradiction:
Adaptability or versatilityVSLoss of information

Solution Approach 1:

The method introduces local asymmetry by incorporating adapters at specific orientations relative to the nucleic acid strand. By using modified nucleotides with pre-coupled adapters that are incorporated in a strand-specific manner, the adapter orientation reflects the original strand direction, preserving strandedness information while maintaining universal adapter compatibility.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach increases yield and simplifies sample preparation by reducing steps, enabling PCR-free or PCR-friendly workflows and maintaining strandedness information, while improving library preparation efficiency.

Implementation Method 1

The modified nucleotide can be used to directly incorporate adapters onto nucleic acids as part of sample preparation for downstream processing steps

Methodology Applied
Scientific EffectPolymerase-mediated reaction: Enzyme

Implementation Method 2

reacting the 5' oligonucleotide end of the oligonucleotide adapter on the extended nucleic acid with the 3' reactive group to couple the 5' oligonucleotide end to the deoxyribose

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 3

cleaving the linker to liberate a 3' end of the oligonucleotide adapter

Methodology Applied
Scientific EffectCleavage: Chemical Bonding

Data Source

PatentEP4347872B1Oligo-modified nucleotide analogues for nucleic acid preparation
Publication Date: 2026.03.25 ILLUMINA INC
  • EP4347872B1 patent drawingFigure 1
  • EP4347872B1 patent drawingFigure 2
  • EP4347872B1 patent drawingFigure 3

AI summary

Nucleic acid techniques are disclosed. Embodiments include modified nucleotides 12 with oligonucleotide adapters 24 that are coupled via cleavable linkers 20. Incorporation of the modified nucleotide 12 at a 3' end of a nucleic acid permits end-adapterization via ligation of a free 5' end of the oligonucleotide adapter 24 to a 3' reactive group of the modified nucleotide 12 and cleavage at the cleavable linker 20 to liberate a free 3' end.