On-Site Titanium Powder Production for Additive Manufacturing

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Solution Overview

Problem

Conventional methods for manufacturing titanium and titanium alloy articles are energy-intensive, wasteful, and involve the use of polluting materials, with a high 'buy-to-fly' ratio and difficulties in recycling due to high oxygen content, leading to increased costs and environmental concerns.

Innovation Solution

An integrated apparatus and method that includes an electrochemical reduction apparatus, a processor, and an additive-manufacturing unit, where the reduction apparatus produces metallic powder on-site just before use in additive manufacturing, reducing waste and eliminating the need for storing metallic powders, and allowing for recycling of oxidized powder to minimize oxygen content.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional Kroll or Hunter processes are used to manufacture titanium sponge, then large-scale production is achieved, but energy consumption increases and polluting materials are used

Engineering Contradiction:
Improveproduction scaleVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSLoss of energy

Solution Approach 1:

The invention changes the chemical parameters of the reduction process by using aluminum thermite reaction instead of conventional chloride-based reduction, operating at lower temperatures (below 2000°C) and producing metallic powder directly rather than sponge, thereby reducing energy consumption while maintaining production capability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the mechanical/chemical intensive Kroll or Hunter processes with an electrochemical reduction system that uses electrical energy to drive the aluminum thermite reaction, substituting chemical reduction with electrochemical reduction to achieve lower energy consumption and direct powder production

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Quantity of substance

If titanium sponge is manufactured using conventional processes, then sufficient material is produced, but the buy-to-fly ratio increases due to substantial material waste during machining

Engineering Contradiction:
Improvematerial availabilityVSAvoidmaterial waste
Core Design Contradiction:
Quantity of substanceVSLoss of substance

Solution Approach 1:

The system produces metallic powder directly at the point of use through electrochemical reduction, eliminating the need for separate machining operations and material transport, thereby self-serving the additive manufacturing process with on-demand powder production and eliminating machining waste

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The invention performs preliminary action by producing the metallic powder directly in the required form for additive manufacturing, preparing the material in advance in the correct state and location, thereby eliminating subsequent machining operations and associated material waste

Inventive Principle:
Principle #10Preliminary action

3Adaptability or versatility

If metallic powder is stored for additive manufacturing, then production flexibility is maintained, but storage hazards increase due to fire risk and degradation

Engineering Contradiction:
Improveproduction flexibilityVSAvoidstorage hazards
Core Design Contradiction:
Adaptability or versatilityVSObject-affected harmful factors

Solution Approach 1:

The system eliminates the need for external powder storage by producing powder on-demand at the additive manufacturing site through electrochemical reduction, making the system self-sufficient and removing the harmful storage hazards while maintaining production flexibility

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The invention introduces an intermediary electrochemical reduction system that acts as a mediator between raw material storage and additive manufacturing, producing powder on-demand and eliminating the need for intermediate powder storage, thereby removing fire risks and degradation concerns

Inventive Principle:
Principle #24Intermediary (Mediator)

4Productivity

If oxidized powder is recycled from additive manufacturing, then material utilization improves, but oxygen content increases making recycling difficult

Engineering Contradiction:
Improvematerial utilizationVSAvoidoxygen content control
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The invention changes the chemical state of recycled powder by subjecting oxidized powder to electrochemical reduction, which removes oxygen and restores the metallic state, thereby enabling recycling while maintaining oxygen content control through the electrochemical process parameters

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces material waste, energy consumption, and storage hazards by producing high-quality metallic powders on-demand, enhancing the efficiency and safety of titanium alloy production while minimizing environmental impact.

Implementation Method 1

a reduction apparatus for electrochemically reducing a feedstock to a metallic product

Methodology Applied
Scientific EffectElectrochemical reduction: Electrolysis

Implementation Method 2

a processor for converting the metallic product to a metallic powder

Methodology Applied
Scientific EffectMechanical comminution: Abrasion

Data Source

PatentEP3464656B1Manufacturing apparatus and method
Publication Date: 2024.01.03 POWER RESOURCES GRP LTD
  • EP3464656B1 patent drawingFigure 1
  • EP3464656B1 patent drawingFigure 2
  • EP3464656B1 patent drawingFigure 3

AI summary

A method and an apparatus for manufacturing a metallic article involve providing a non- metallic feedstock, for example in the form of an oxide of a desired metal or a mixture of oxides of the components of a desired metal alloy. A manufacturing apparatus has a reduction apparatus for electrochemically reducing the feedstock to a metallic product and a processor for converting the metallic product to a metallic powder. The powder is fed into an additive-manufacturing apparatus for fabricating the metallic article from the metallic powder. At least the reduction apparatus and the processor, and preferably also the additive-manufacturing apparatus, are collocated, or located in the same container, or in the same building, or on the same site.