Optical Analysis Apparatus Bubble Segmentation Flow

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Solution Overview

Problem

Existing methods for measuring the composition of substances in reaction vessels face challenges such as contamination, changes in composition due to gas, liquid, or solid additions, and difficulty in performing continuous measurements without mixing samples, leading to inaccurate analysis.

Innovation Solution

An optical analysis apparatus with a flow passage system that introduces bubbles to divide the substance, allowing for precise measurement by irradiating the substance and bubbles with light, thereby preventing mixing and ensuring accurate analysis at the sampling time.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If the substance is extracted using an instrument such as a dropper or syringe, then measurement can be performed, but continuous measurement is difficult and contamination or composition changes occur

Engineering Contradiction:
Improvemeasurement accuracyVSAvoidcontinuous measurement capability
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The substance flow is segmented into discrete portions by introducing bubbles that divide the continuous flow into separate segments. Each segment contains a specific sample taken at a specific time, allowing continuous measurement without mixing between samples while maintaining measurement accuracy.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Bubbles are introduced as an intermediary substance to divide and separate the liquid flow. The bubbles act as physical barriers that prevent mixing between different samples while allowing the measurement to proceed continuously through the flow passage.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Quantity of substance

If the lid of the vessel is opened to extract the substance, then the substance can be sampled, but gas is released or air enters causing composition changes or contamination

Engineering Contradiction:
Improvesubstance samplingVSAvoidcontamination and composition change
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The harmful effect of opening the lid is eliminated by extracting only the necessary function (substance sampling) through the closed lid structure. Sampling ports or injection points are provided in the lid, allowing substance extraction without opening the vessel, thus preventing contamination and composition changes.

Inventive Principle:
Principle #2Taking out (Extraction)

3Productivity

If the substance is circulated through flow passages, then continuous measurement is possible, but samples taken at different times mix together causing inaccurate analysis

Engineering Contradiction:
Improvecontinuous measurement capabilityVSAvoidanalysis accuracy at sampling time
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The continuous flow in the flow passage is segmented into discrete portions by introducing bubbles. Each bubble divides the flow, creating separate segments that contain samples from specific time points. This segmentation prevents mixing between samples while allowing continuous circulation and measurement.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Bubbles are introduced periodically into the flow passage at regular intervals to divide the continuous substance flow. This periodic introduction of dividing elements ensures that samples taken at different times remain separated, maintaining analysis accuracy while enabling continuous measurement.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate analysis of the substance's composition at the sampling time by preventing contamination and mixing, even when the vessel's composition changes, ensuring reliable measurement data.

Implementation Method 1

a measurement unit, which is provided to the flow passage, and is configured to perform measurement by irradiating the first substance and the second substances flowing through the flow passage with light

Methodology Applied
Scientific EffectLight absorption: Absorption (EM radiation)

Data Source

PatentUS10801949B2Optical analysis apparatus and manufacturing system for a substance
Publication Date: 2020.10.13 HITACHI LTD
  • US10801949B2 patent drawing
  • US10801949B2 patent drawing
  • US10801949B2 patent drawing

AI summary

To perform more accurate analysis of a composition of a substance given at a sampling time, provided is an optical analysis apparatus, including: a flow passage, which is connected to a vessel, and is configured to allow a first substance to flow therethrough; an introduction unit, which is provided to the flow passage, and is configured to introduce at least two second substances to the flow passage, to thereby divide the first substance flowing through the flow passage; and a measurement unit, which is provided to the flow passage, and is configured to perform measurement by irradiating the first substance and the second substance flowing through the flow passage with light.