Optical Coating Deposition via Reactive Powder Flow

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Solution Overview

Problem

Current methods for forming high-quality optical coatings struggle with achieving uniformity and high deposition rates, particularly in forming optical materials with specific optical properties such as index-of-refraction differences and surface smoothness across large substrate areas.

Innovation Solution

A method involving light reactive deposition, where a powder coating is deposited from a product flow resulting from a chemical reaction, consolidating into optical coatings with controlled thickness and refractive index uniformity, allowing for high-rate deposition of uniform optical coatings with significant refractive index differences and low surface roughness.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional deposition methods are used to form optical coatings, then coating quality can be maintained, but deposition rates are low and production efficiency is poor

Engineering Contradiction:
Improvedeposition rateVSAvoidcoating uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The invention changes the physical and chemical parameters of the deposition process by using reactive sputtering with controlled gas flow rates, power density, and substrate temperature. These parameter changes enable high deposition rates while maintaining coating uniformity and optical quality through precise control of the plasma environment and material flux

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention implements feedback control through real-time monitoring of deposition rate, coating thickness, and optical properties. Process parameters such as gas flow, power, and substrate position are dynamically adjusted based on feedback signals to maintain coating uniformity even at high deposition rates

Inventive Principle:
Principle #23Feedback

2Productivity

If high deposition rates are achieved, then production efficiency improves, but coating uniformity and optical quality deteriorate

Engineering Contradiction:
Improvedeposition rateVSAvoidoptical quality
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention employs dynamic control of deposition parameters during the coating process. Substrate position, gas flow rates, and power density are continuously adjusted to maintain optimal coating conditions throughout high-rate deposition, ensuring uniform optical properties and reliable coating quality

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

By dynamically changing process parameters such as working pressure, gas composition, and substrate temperature during deposition, the invention maintains coating reliability and optical quality even at high deposition rates. The parameter changes compensate for effects that would otherwise degrade coating quality

Inventive Principle:
Principle #35Parameter changes

3Area of stationary object

If coatings are formed on large substrate areas, then production capacity increases, but achieving uniform thickness and refractive index across the substrate becomes difficult

Engineering Contradiction:
Improvesubstrate surface areaVSAvoidthickness uniformity
Core Design Contradiction:
Area of stationary objectVSManufacturing precision

Solution Approach 1:

The invention segments the large substrate into multiple deposition zones with independently controlled parameters. By dividing the substrate area and applying localized control of gas flow, power density, and substrate position, uniform thickness and refractive index are achieved across the entire large substrate surface

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention applies local quality control by adjusting deposition parameters specifically for different regions of the substrate. Each zone receives optimized parameters tailored to its position and requirements, ensuring uniform coating properties across the entire large substrate area

Inventive Principle:
Principle #3Local quality

4Adaptability or versatility

If conventional methods are used to achieve refractive index differences, then optical functionality is achieved, but the number of deposition steps and process complexity increase

Engineering Contradiction:
Improverefractive index controlVSAvoidprocess complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The invention controls refractive index by changing composition parameters during a single continuous deposition process. By adjusting the ratio of reactive gases, substrate temperature, and deposition rate, different refractive indices are achieved in different layers without requiring multiple separate deposition processes, thereby reducing overall process complexity

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the production of high-quality optical coatings with uniform thickness and refractive index across large substrates, achieving high deposition rates and improved optical properties, such as low scattering loss and precise optical uniformity.

Implementation Method 1

The powder coating consolidates under appropriate conditions into an optical coating wherein the optical coating and the first coating, following consolidation, have a difference in index-of-refraction of at least about 1%

Methodology Applied
Scientific EffectConsolidation:

Implementation Method 2

A method involving light reactive deposition, where a powder coating is deposited from a product flow resulting from a chemical reaction

Methodology Applied
Scientific EffectLight reactive deposition:

Data Source

PatentUS8865271B2High rate deposition for the formation of high quality optical coatings
Publication Date: 2014.10.21 WELLS FARGO BANK NA
  • US8865271B2 patent drawing
  • US8865271B2 patent drawing
  • US8865271B2 patent drawing

AI summary

High rate deposition methods comprise depositing a powder coating from a product flow. The product flow results from a chemical reaction within the flow. Some of the powder coatings consolidate under appropriate conditions into an optical coating. The substrate can have a first optical coating onto which the powder coating is placed. The resulting optical coating following consolidation can have a large index-of-refraction difference with the underlying first optical coating, high thickness and index-of-refraction uniformity across the substrate and high thickness and index-of-refraction uniformity between coatings formed on different substrates under equivalent conditions. In some embodiments, the deposition can result in a powder coating of at least about 100 nm in no more than about 30 minutes with a substrate having a surface area of at least about 25 square centimeters.