Optical Fiber Preform Plasma Deposition Layer Cracking

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Solution Overview

Problem

Current plasma deposition processes for manufacturing optical fiber preforms result in irregular glass deposition leading to soot rings, which cause layer cracking and fracture, especially as preforms become larger and thicker, reducing the effective length and increasing the risk of fracture.

Innovation Solution

A method involving the creation of distinct plasma reaction zones with different conditions for depositing non-vitrified and vitrified silica layers, where non-vitrified layers are deposited at reversal points and subsequently vitrified or etched, reducing tension between layers and preventing crack propagation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Volume of moving object

If the substrate tube is larger and thicker to enable larger preforms, then the preform size increases, but the risk of layer cracking and fracture increases

Engineering Contradiction:
Improvepreform sizeVSAvoidrisk of layer cracking
Core Design Contradiction:
Volume of moving objectVSReliability

Solution Approach 1:

The patent changes the deposition parameters by creating distinct plasma reaction zones with different conditions - a first zone for depositing non-vitrified silica layers and a second zone for depositing vitrified silica layers. This parameter differentiation allows control over layer structure and stress distribution, preventing cracking in larger preforms while maintaining the ability to produce bigger sizes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent utilizes phase transitions of silica by depositing non-vitrified silica layers in the first plasma reaction zone and then vitrifying them in the second plasma reaction zone. This controlled phase transition from non-vitrified to vitrified state allows the layers to set properly without excessive tension, preventing cracks in larger preform structures.

Inventive Principle:
Principle #36Phase transitions

2Ease of manufacture

If regular plasma deposition is used, then the deposition process is simple, but soot rings form causing layer cracking

Engineering Contradiction:
Improvedeposition process simplicityVSAvoidglass layer uniformity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent segments the single plasma deposition process into two distinct plasma reaction zones: a first zone for non-vitrified silica deposition and a second zone for vitrified silica deposition. This segmentation prevents the formation of soot rings by separating the deposition stages, maintaining manufacturing precision while keeping the overall process relatively simple.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent introduces an intermediary non-vitrified silica layer between the substrate and the final vitrified glass layers. This intermediary layer acts as a buffer that prevents direct contact between the substrate and subsequent glass layers, eliminating the tension that causes cracking at soot ring locations while maintaining process simplicity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Strength

If non-vitrified silica layers are deposited at reversal points, then layer tension is reduced, but an additional deposition step is required

Engineering Contradiction:
Improvelayer tension resistanceVSAvoiddeposition process steps
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent merges the deposition of non-vitrified and vitrified silica layers into a single continuous plasma deposition process with two distinct reaction zones. This combining approach reduces layer tension by controlling the deposition sequence while avoiding the need for separate processing steps, thereby not increasing device complexity despite the additional functional step.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach minimizes layer cracking, maintains preform integrity, and allows for longer, thicker preforms with reduced risk of fracture, enabling more efficient production of optical fibers.

Implementation Method 1

method for manufacturing a precursor for a primary preform for optical fibres by means of an internal plasma deposition process, such as a plasma chemical vapour deposition (PCVD) process

Methodology Applied
Scientific EffectPlasma-enhanced chemical vapour deposition: Plasma Enhanced Chemical Vapour Deposition

Implementation Method 2

Plasma-enhanced chemical vapour deposition (PECVD or PCVD) is a process used to deposit thin films from a gas state (vapour) to a solid state on a substrate

Methodology Applied
Scientific EffectChemical vapour deposition: Chemical Vapour Deposition

Implementation Method 3

the plasma is induced by the use of electromagnetic radiation, e.g. microwaves. Generally, electromagnetic radiation from a generator is directed towards an applicator via a waveguide

Methodology Applied
Scientific EffectElectromagnetic radiation plasma generation: Electromagnetic Induction

Implementation Method 4

The applicator and the substrate tube are generally surrounded by a furnace so as to maintain the substrate tube at a temperature of 900-1300° C. during the deposition process

Methodology Applied
Scientific EffectThermal heating: Heating

Implementation Method 5

The removal is optionally carried out by means of a vacuum pump. The vacuum pump has the effect of generating a reduced pressure in the interior of the substrate tube

Methodology Applied
Scientific EffectVacuum pumping: Vacuum

Data Source

PatentUS9643879B2Method for manufacturing a precursor for a primary preform for optical fibres by a plasma deposition process
Publication Date: 2017.05.09 DRAKA COMTEQ BV

AI summary

A method for manufacturing a precursor for a primary preform for optical fibers by an internal plasma deposition process including the steps of providing a hollow substrate tube, creating a first plasma reaction zone having first reaction conditions and depositing non-vitrified silica layers along at least a portion of the inner surface of the substrate tube, subsequently creating a second plasma reaction zone having second reaction conditions different from the first reaction conditions and depositing vitrified silica layers along at least a portion of the substrate tube, and cooling the substrate tube to produce the precursor for a primary preform.