Optical Glass Composition for High Index and Devitrification Stability

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Solution Overview

Problem

Existing optical glasses lack the flexibility to achieve high refractive index, high transmittance, and devitrification resistance stability, limiting their application in advanced optical systems and devices.

Innovation Solution

An optical glass composition comprising 5% to 35% La3+, 5% to 25% Si4+, 5% to 35% Nb5+, 5% to 35% Al3+, and 45% to 80% of a total content rate of Ti4+, Zr4+, Nb5+, Ta5+, and Al3+, manufactured using a floating melting method to avoid crucible contact, ensuring high refractive index, transmittance, and devitrification resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If conventional optical glass compositions are used, then manufacturing is simpler, but refractive index and transmittance cannot be sufficiently increased

Engineering Contradiction:
Improverefractive indexVSAvoidmanufacturing complexity
Core Design Contradiction:
TemperatureVSEase of manufacture

Solution Approach 1:

The patent applies parameter changes by systematically adjusting the chemical composition parameters of the optical glass, specifically setting La3+ content at 5-35 mol%, Nb5+ at 5-35 mol%, and the ratio of (Ti4+ + Zr4+) to total cations at 45-80%, to achieve the target refractive index of 1.95-2.15 and transmittance of 80% at 420nm or less

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by combining multiple metal oxides (La2O3, Nb2O5, TiO2, ZrO2, Al2O3, SiO2, B2O3) in specific proportions to create a new optical glass composition that achieves high refractive index and transmittance properties that cannot be obtained with conventional single-component or simple composite glasses

Inventive Principle:
Principle #40Composite materials

2Adaptability or versatility

If high refractive index glass is developed, then optical system design flexibility increases, but devitrification resistance stability deteriorates

Engineering Contradiction:
Improveoptical system design flexibilityVSAvoiddevitrification resistance stability
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters by incorporating specific amounts of Al3+ (5-35 mol%) and controlling the ratio of high-field-strength cations (Ti4+, Zr4+, Nb5+, Ta5+) to total cations at 45-80%, which enhances devitrification resistance while maintaining the high refractive index needed for optical system design flexibility

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses Al2O3 and SiO2 as intermediary components that mediate between the high refractive index requirements (from La2O3 and Nb2O5) and devitrification resistance stability, acting as network formers and stabilizers that prevent crystallization while allowing the optical properties to be optimized

Inventive Principle:
Principle #24Intermediary (Mediator)

3Ease of manufacture

If crucible melting method is used, then manufacturing process is simpler, but glass purity and transmittance are compromised

Engineering Contradiction:
Improvemanufacturing process simplicityVSAvoidglass purity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent extracts the glass from contact with crucible materials by using a floating melting method where the molten glass floats on a protective flux layer, eliminating contamination from crucible walls and achieving the high purity required for 80% transmittance at 420nm or less

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces a protective flux layer as an intermediary between the molten glass and the crucible, preventing direct contact and contamination while still allowing heat transfer for melting, thus maintaining both manufacturing feasibility and glass purity

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The optical glass achieves a refractive index of 1.95 to 2.15, transmittance of 80% at 420 nm or less, and devitrification resistance with a temperature difference of 80°C to 200°C, enabling stable production of large glass gobs for advanced optical elements and systems.

Implementation Method 1

an optical glass having a high refractive index has been required

Methodology Applied
Scientific EffectRefraction: Refraction

Implementation Method 2

manufactured using a floating melting method to avoid crucible contact

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 3

devitrification resistance stability deteriorates

Methodology Applied
Scientific EffectDevitrification resistance: Vitrification

Data Source

PatentEP4596508A1Optical glass, optical element, optical system, cemented lens, objective lens for microscope, interchangeable lens for camera, and optical device
Publication Date: 2025.08.06 NIKON CORP
  • EP4596508A1 patent drawingFigure 1~2
  • EP4596508A1 patent drawingFigure 3~4
  • EP4596508A1 patent drawingFigure 5~6

AI summary

An optical glass includes, by mol% of a cation, 5% to 35% of a content rate of La3+; 5% to 25% of a content rate of Si4+; 5% to 35% of a content rate of Nb5+; 5% to 35% of a content rate of Al3+; and 45% to 80% of a total content rate of Ti4+, Zr4+, Nb5+, Ta5+, and Al3+ (Ti4+ + Zr4+ + Nb5+ + Ta5+ + Al3+).