Orange Juice Ultrafiltration and Selective Pasteurization

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Solution Overview

Problem

Existing methods for producing orange juice fail to maintain the natural flavor and quality of freshly squeezed juice while extending its shelf life, as they typically involve direct pasteurization that compromises flavor and aroma components.

Innovation Solution

A method involving a single membrane filtration step using a ceramic ultrafilter with a pore size of 19-21 nm, where raw orange juice is ultrafiltered to produce a permeate and retentate, and only the retentate is pasteurized, minimizing heat treatment and preserving flavor components in the permeate.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of stationary object

If direct pasteurization of raw orange juice is used, then shelf life is extended, but flavor and aroma components are compromised

Engineering Contradiction:
Improveshelf lifeVSAvoidloss of flavor and aroma
Core Design Contradiction:
Duration of action of stationary objectVSObject-generated harmful factors

Solution Approach 1:

The orange juice is divided into two fractions through ultrafiltration: permeate containing flavor and aroma components, and retentate containing enzymes and microorganisms. This segmentation allows selective treatment of each fraction - the permeate remains untreated to preserve flavor, while the retentate is pasteurized to extend shelf life.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The harmful enzymes and microorganisms are extracted from the orange juice by separating them into the retentate fraction through ultrafiltration. This extraction allows the harmful components to be removed from the final product while the beneficial flavor components remain in the permeate.

Inventive Principle:
Principle #2Taking out (Extraction)

2Manufacturing precision

If multiple membrane filtration steps are used, then purification is improved, but process complexity increases

Engineering Contradiction:
Improvepurification levelVSAvoidnumber of filtration steps
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

A single ultrafiltration membrane performs multiple functions simultaneously: it separates enzymes, microorganisms, and flavor components in one step. This multi-functionality eliminates the need for multiple sequential filtration steps while achieving the required purification level.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent combines enzyme removal, microorganism removal, and flavor component separation into a single ultrafiltration step. By merging these functions into one process, the overall complexity is reduced while maintaining effective purification.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in orange juice with improved flavor and quality, retaining over 95% of vitamin C, essential oils, and lactic bacteria CFU, while achieving a shelf life similar to not-from-concentrate (NFC) orange juice, with less than 1% enzyme pectin esterase content and a significant reduction in detrimental microorganisms.

Implementation Method 1

The cooled raw orange juice is ultrafiltrated by a ceramic type ultrafilter having a membrane with a pore size of 19-21 nm and a channel size of 3.5-4.5 mm to produce a permeate and a retentate

Methodology Applied
Scientific EffectUltrafiltration: Semipermeable Membrane

Implementation Method 2

Production, starting from freshly squeezed orange juice (often referred to as raw orange juice), of an orange juice product that has a natural flavor while at the same time maximizing the shelf life

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 3

The retentate is pasteurized and then mixed with the permeate to produce orange juice having an enzyme pectin esterase (PEU) content that is less than 1 % of the PEU content of the raw orange juice

Methodology Applied
Scientific EffectPasteurization: Heating

Data Source

PatentEP3628171B1Production of orange juice
Publication Date: 2024.10.30 TETRA LAVAL HOLDINGS & FINANCE SA
  • EP3628171B1 patent drawingFigure 1
  • EP3628171B1 patent drawingFigure 2

AI summary

Production of orange juice (108) is described. Raw orange juice (102) is ultrafiltrated in an ultrafilter (107), thereby obtaining a retentate (106) and a permeate (104). Only the retentate (106) is pasteurized in a pasteurizer (113). The pasteurized retentate (106) and the permeate (104) is mixed in a mixing unit (109). A minimization of enzymes and microorganisms is thereby obtained in the orange juice (108).