Organic Photoelectric Conversion Device with Electron Blocking Layer

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Solution Overview

Problem

Conventional photoelectric conversion devices for solid-state imaging suffer from reduced sensitivity and increased dark current due to small pixel size, heat resistance issues, and inadequate charge transportability, particularly when used in imaging devices that require high photoelectric conversion efficiency and heat resistance.

Innovation Solution

A photoelectric conversion device with a specific compound structure, comprising a transparent electrically conductive film, a photoelectric conversion layer containing a fullerene or fullerene derivative, and an electron blocking layer with a compound represented by formula (F-1), which enhances charge transportability and reduces dark current even under high temperature conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If the pixel size is reduced to increase the number of pixels, then the resolution is improved, but the aperture ratio and light collection efficiency are reduced

Engineering Contradiction:
ImproveresolutionVSAvoidaperture ratio
Core Design Contradiction:
Measurement precisionVSQuantity of substance

Solution Approach 1:

The patent changes the material parameter of the photoelectric conversion layer from conventional inorganic materials to organic materials with specific molecular structures (containing carbazole, triphenylamine, or xylene groups). This material parameter change enables high photoelectric conversion efficiency even in small pixel areas, effectively resolving the contradiction between high resolution and sufficient light collection efficiency.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If a voltage is externally applied to enhance photoelectric conversion efficiency and response speed, then the photoelectric conversion efficiency is improved, but the dark current increases due to charge injection from electrodes

Engineering Contradiction:
Improvephotoelectric conversion efficiencyVSAvoiddark current
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent changes the energy level parameters of the photoelectric conversion layer by selecting organic materials with specific HOMO and LUMO levels. The HOMO level is set higher than the electrode work function (4.5-5.0 eV) and the LUMO level is set lower than the electrode work function, creating energy barriers that prevent charge injection while maintaining efficient photoelectric conversion.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces the organic photoelectric conversion layer as an intermediary between the electrode and the photoelectric conversion process. This intermediate layer with specifically tuned energy levels acts as a buffer that allows efficient exciton dissociation while blocking direct charge injection from the electrode, thus reducing dark current.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If conventional organic photoelectric conversion materials are used, then the photoelectric conversion efficiency is improved, but the heat resistance is insufficient for high temperature processing

Engineering Contradiction:
Improvephotoelectric conversion efficiencyVSAvoidheat resistance
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The patent changes the thermal stability parameters of the organic materials by selecting compounds with high glass transition temperatures (Tg > 100°C) and high decomposition temperatures. Specific molecular structures containing carbazole, triphenylamine, or xylene groups are chosen to achieve both high photoelectric conversion efficiency and sufficient heat resistance for high temperature processing.

Inventive Principle:
Principle #35Parameter changes

4Measurement precision

If the pixel size is reduced, then the resolution is improved, but the sensitivity is reduced due to reduced light collection efficiency

Engineering Contradiction:
ImproveresolutionVSAvoidsensitivity
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent changes the photoelectric conversion parameters of the material by using organic materials with high exciton dissociation efficiency and appropriate energy levels. This enables small pixels to maintain high sensitivity despite reduced light collection area, as the organic photoelectric conversion layer efficiently converts the collected light into electrical signals.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device achieves low dark current and improved heat resistance, maintaining high photoelectric conversion efficiency and response speed, even during heat treatment processes, making it suitable for imaging devices.

Implementation Method 1

photoelectric conversion layer containing a fullerene or fullerene derivative

Methodology Applied
Scientific EffectPhotoelectric conversion: Photovoltaic Effect

Implementation Method 2

a technique of providing a charge blocking layer to suppress the injection of an electric charge into the photoelectric conversion layer

Methodology Applied
Scientific EffectCharge blocking: Electrostatics

Data Source

PatentEP2306541B1Photoelectric conversion device, production method thereof, photosensor, imaging device and their drive methods
Publication Date: 2018.10.24 FUJIFILM CORP
  • EP2306541B1 patent drawingFigure 1A~1B
  • EP2306541B1 patent drawingFigure 2
  • EP2306541B1 patent drawing

AI summary

A photoelectric conversion device comprising a transparent electrically conductive film, a photoelectric conversion film and an electrically conductive film in this order, wherein the photoelectric conversion film comprises a photoelectric conversion layer, and an electron blocking layer, wherein the electron blocking layer contains a compound represented by the specific formula.