OSA Starch Emulsification for High-Fat Spray-Dried Powders

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Solution Overview

Problem

Existing spray drying processes struggle with high-fat and high-carbohydrate compositions due to issues like increased free fat content, caking, and viscosity, leading to reduced production efficiency and component degradation.

Innovation Solution

Employing octenylsuccinyl anhydride substituted starch (OSA starch) as an emulsifier to increase the dry weight and fat content in liquid compositions, allowing for lower free fat content in the spray-dried powder, thereby enabling dry blending of additional components without high-pressure or high-temperature exposure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If the fat content in the liquid composition is increased to improve nutritional value and reduce production costs, then the production efficiency decreases and free fat content increases due to caking and swelling

Engineering Contradiction:
Improvefat contentVSAvoidproduction efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

OSA starch acts as an intermediary substance that mediates between fat and water phases. The modified starch with octenyl succinic anhydride groups provides steric stabilization and electrostatic repulsion, preventing fat droplet coalescence and caking during spray drying. This allows high fat content (up to 80 wt% or more) to be maintained without the harmful effects of free fat separation.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the chemical parameters of the starch by modifying it with octenyl succinic anhydride, transforming ordinary starch into OSA starch with enhanced emulsifying properties. This parameter change enables the starch to stabilize high-fat emulsions that would otherwise be unstable, resolving the contradiction between high fat content and production efficiency.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the carbohydrate content is increased to improve nutritional value, then the viscosity increases and caking occurs, requiring further dilution that reduces production efficiency

Engineering Contradiction:
Improvecarbohydrate contentVSAvoidproduction efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The invention uses a composite system where OSA starch (modified carbohydrate) combines emulsifying, thickening, and stabilizing properties. The octenyl succinic anhydride modification creates a composite material that maintains low viscosity even at high carbohydrate concentrations while preventing caking, eliminating the need for dilution and preserving production efficiency.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

By modifying the carbohydrate (starch) with octenyl succinic anhydride, the invention changes its physical and chemical parameters including solubility, viscosity, and emulsifying capacity. This parameter transformation allows high carbohydrate content to be maintained without the adverse effects of caking and excessive viscosity.

Inventive Principle:
Principle #35Parameter changes

3Stability of the object's composition

If conventional emulsifiers are used to stabilize high-fat compositions, then the emulsion stability improves, but the free fat content exceeds the acceptable limit of 3 wt%

Engineering Contradiction:
Improveemulsion stabilityVSAvoidfree fat content
Core Design Contradiction:
Stability of the object's compositionVSObject-generated harmful factors

Solution Approach 1:

OSA starch serves as an intermediary emulsifier that creates a stable interface between fat and water phases. The modified starch molecules with hydrophobic octenyl groups and hydrophilic starch backbones form a protective barrier around fat droplets, preventing coalescence and reducing free fat content to below 3 wt% while maintaining emulsion stability.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention changes the emulsifying parameters by using OSA starch instead of conventional emulsifiers. The unique molecular structure of OSA starch with its specific hydrophobic-hydrophilic balance provides superior emulsifying performance that simultaneously achieves high stability and low free fat content, resolving the contradiction between these two parameters.

Inventive Principle:
Principle #35Parameter changes

4Use of energy by moving object

If the liquid composition is highly concentrated to reduce water removal requirements, then the energy consumption decreases, but the viscosity increases making spray drying difficult

Engineering Contradiction:
Improveenergy consumptionVSAvoidspray drying handleability
Core Design Contradiction:
Use of energy by moving objectVSEase of operation

Solution Approach 1:

The invention changes the rheological parameters of the liquid composition by using OSA starch as a stabilizer. The modified starch maintains low viscosity and good flow properties even at high solid concentrations, allowing the composition to be sprayed easily while requiring minimal water removal and thus low energy consumption.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

OSA starch acts as an intermediary that facilitates the interaction between high concentration solids and the spray drying process. It prevents excessive viscosity buildup and maintains sprayability, enabling highly concentrated compositions to be processed efficiently with low energy input.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of OSA starch results in powders with less than 3 wt% free fat, improving sensorial properties and process efficiency by reducing energy consumption, fouling, and allowing for greater flexibility in formulating nutritional products.

Implementation Method 1

Employing octenylsuccinyl anhydride substituted starch (OSA starch) as an emulsifier to increase the dry weight and fat content in liquid compositions

Methodology Applied
Scientific EffectEmulsion: Emulsion

Implementation Method 2

Process for preparing powders by spray drying

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS12446606B2Process for preparing powders by spray drying and powders obtainable thereby
Publication Date: 2025.10.21 NV NUTRICIA
  • US12446606B2 patent drawing

AI summary

The present invention relates to a use of octenylsuccinyl anhydride substituted starch (OSA starch) for increasing the dry weight content and/or the fat content of a liquid composition that is subjected to a spray-drying step, and also to a process for preparing powders. The present invention enables the spray-drying of emulsions that contain a high amount of fat. The present invention also relates to the powder products obtainable by the process and nutritional products such as an infant milk powder, grow up milk, toddler milk or as a medical nutritional product that can be formulated therewith.