Oxidative method for decolorizing textile materials

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Solution Overview

Problem

Current recycling methods for synthetic fiber textiles are hindered by the presence of colorants, which require costly and complex depolymerization and repolymerization steps, and existing wastewater treatment processes are not efficient in selectively removing colorants from polymer materials without degrading the polymers.

Innovation Solution

A method using a Fenton's reagent, comprising hydrogen peroxide and an iron catalyst, combined with a ketone such as acetone, to decolorize synthetic polymer materials like polyester textiles without significant degradation, by treating them at a pH of 4 or less and temperatures above 50°C, effectively removing colorants while preserving the polymer structure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-generated harmful factors

If depolymerization and repolymerization steps are used to remove colorants, then colorant removal is achieved, but process cost and complexity increase significantly

Engineering Contradiction:
Improvecolorant removalVSAvoidprocess complexity
Core Design Contradiction:
Object-generated harmful factorsVSDevice complexity

Solution Approach 1:

The patent extracts and removes only the colorant component from the polymer material using selective chemical treatment, while leaving the polymer structure intact. This avoids the need for complete depolymerization and repolymerization, thereby simplifying the process while achieving colorant removal.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent employs parameter changes by adjusting pH levels and using specific chemical reagents to selectively target and remove colorants without affecting the polymer. This selective approach based on chemical parameter manipulation eliminates the need for complex depolymerization- repolymerization cycles.

Inventive Principle:
Principle #35Parameter changes

2Object-generated harmful factors

If conventional wastewater treatment processes are used to remove colorants, then colorant removal is attempted, but polymer degradation occurs

Engineering Contradiction:
Improvecolorant removalVSAvoidpolymer structure stability
Core Design Contradiction:
Object-generated harmful factorsVSStability of the object's composition

Solution Approach 1:

The patent applies local quality by using selective chemical treatment that targets only the colorant molecules with specific chemical properties, while the polymer material remains unaffected. This localized chemical action ensures colorant removal without compromising polymer structure stability.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent introduces chemical intermediaries (specific reagents and pH conditions) that facilitate selective colorant removal. These intermediaries interact preferentially with colorants rather than the polymer, enabling colorant extraction while preserving polymer integrity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If colorants are present in recycled synthetic fibers, then recycling can proceed, but commercial attractiveness is reduced

Engineering Contradiction:
Improverecycling efficiencyVSAvoidcommercial attractiveness
Core Design Contradiction:
ProductivityVSEase of manufacture

Solution Approach 1:

The patent performs preliminary colorant removal treatment on recycled synthetic fibers before they enter the main recycling process. This preliminary decolorization step enhances the commercial value of recycled materials, making them more attractive for manufacturing applications while maintaining recycling efficiency.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method achieves significant decolorization of synthetic polymers with minimal impact on their structure, allowing for the recycling and reuse of textiles, as evidenced by reduced K/S values and minimal changes in intrinsic viscosity and molecular weight.

Implementation Method 1

treating a dye-colored synthetic polymer with a treatment composition, the treatment composition comprising (a) hydrogen peroxide, (b) an iron-containing catalyst

Methodology Applied
Scientific EffectFenton's reagent: Oxidation

Implementation Method 2

oxidative method for decolorizing textile materials

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 3

the treating is carried out at a temperature of at least 50° C.

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 4

an iron-containing catalyst

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentUS11001961B2Oxidative method for decolorizing textile materials
Publication Date: 2021.05.11 NORTH CAROLINA STATE UNIV

AI summary

The disclosure relates to a method for decolorization of a dye-colored synthetic polymer, which includes the steps of treating a dye-colored synthetic polymer, such as polyester, with a treatment composition at pH 4 or less, the treatment composition comprising hydrogen peroxide, an iron catalyst, water, and a ketone. The resulting decolorized synthetic polymer is then separated from the treatment composition.