Oxide-Coated High-Strength Bolt for Stable Fastening Axial Force

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Solution Overview

Problem

High-strength bolts, particularly those made of high-carbon steel with silicon, face challenges in maintaining consistent fastening axial force due to varying friction levels and surface treatments that can lead to delayed fracture and reduced fatigue strength.

Innovation Solution

A high-carbon steel bolt with a composition of 0.50-0.65% C, 1.5-2.5% Si, 1.0-2.0% Cr, 0.2-1.0% Mn, and 1.5-5.0% Mo, coated with an iron-based oxide film of 3-20 μm thickness, formed through heat treatment to prevent defects and ensure reliable fastening axial force.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If high-carbon steel with silicon is used to increase tensile strength and delayed fracture resistance, then strength and delayed fracture resistance are improved, but fastening axial force varies greatly with tightening torque due to friction variations

Engineering Contradiction:
Improvetensile strength and delayed fracture resistanceVSAvoidfastening axial force consistency
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The invention changes the surface friction parameter by forming an iron-based oxide film with controlled thickness (3-20 μm) and composition (Fe, FeO, Fe3O4, Fe2O3). This modifies the surface properties to reduce friction coefficient and its variation, making fastening axial force less sensitive to tightening torque variations while maintaining the high strength properties of the silicon-containing steel material.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The iron-based oxide film acts as an intermediary layer between the high-carbon steel bolt surface and the mating fastened member. This intermediate oxide layer mediates the friction interaction, providing a stable friction characteristic that reduces the direct contact friction variations between the high-strength steel surfaces, thereby stabilizing the fastening axial force.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If surface treatment such as chromium plating or phosphoric acid film is applied to prevent galling and stabilize fastening, then fastening properties are improved, but hydrogen invasion occurs causing delayed fracture and surface roughness decreases fatigue strength

Engineering Contradiction:
Improvefastening property stabilityVSAvoiddelayed fracture and fatigue strength reduction
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention uses an iron-based oxide film that can be formed directly on the bolt surface through controlled oxidation, replacing complex multi-layer plating systems. This simpler oxide film provides sufficient friction control and protection without creating the hydrogen trapping issues associated with phosphoric acid films or chromium plating, effectively using a simpler, shorter-process solution.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The invention converts the naturally occurring oxide layer on the steel surface, which would normally be considered a surface defect or contamination, into a beneficial functional layer. By controlling the oxide film thickness to 3-20 μm and composition, the naturally formed oxide that would otherwise be harmful is transformed into a protective layer that reduces friction and stabilizes fastening properties without inviting hydrogen invasion.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Force

If tightening torque is increased to secure fastening axial force, then fastening axial force is improved, but friction loss increases and fastening axial force varies due to surface roughness and lubrication state

Engineering Contradiction:
Improvefastening axial forceVSAvoidfriction loss
Core Design Contradiction:
ForceVSLoss of energy

Solution Approach 1:

The invention changes the surface friction parameter by forming an iron-based oxide film with controlled thickness (3-20 μm) and composition (Fe, FeO, Fe3O4, Fe2O3). This modifies the surface properties to reduce friction coefficient and its variation, making fastening axial force less sensitive to tightening torque variations while maintaining the high strength properties of the silicon-containing steel material.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The iron-based oxide film provides excellent delayed fracture resistance and consistent fastening axial force by minimizing friction and preventing film defects, enhancing both strength and reliability of the bolt.

Implementation Method 1

a friction coefficient of the bolt is changed and variation of a fastening axial force is generated

Methodology Applied
Scientific EffectFriction: Friction

Implementation Method 2

The delayed fracture is a kind of environmental embrittlement that occurs by mutual interaction among material, environment, and stress. It is considered that the delayed fracture is due to embrittlement of material caused by hydrogen.

Methodology Applied
Scientific EffectHydrogen embrittlement resistance: Absorption (physical)

Data Source

PatentUS11708622B2Bolt and fastened structure
Publication Date: 2023.07.25 NISSAN MOTOR CO LTD
  • US11708622B2 patent drawing

AI summary

A bolt of the present invention has a composition comprising: 0.50 mass % or greater and 0.65 mass % or less of carbon (C), 1.5 mass % or greater and 2.5 mass % or less of silicon (Si), 1.0 mass % or greater and 2.0 mass % or less of chromium (Cr), 0.2 mass % or greater and 1.0 mass % or less of manganese (Mn), 1.5 mass % or greater and 5.0 mass % or less of molybdenum (Mo), wherein a total amount of phosphorous (P) and sulfur (S) as impurities is 0.03 mass % or less, the remaining is iron (Fe), and the bolt comprises an iron based oxide film with a film thickness of 3 μm or greater and 20 μm or less on the surface thereof. The bolt has excellent delayed fracture resistance and reliably provides a fastening axial force.