Oxygen Nanobubble Oxidation for 1,4-Dioxane Removal

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Solution Overview

Problem

Conventional water treatment processes struggle to effectively remove recalcitrant contaminants such as 1,4-dioxane and PPCPs due to high chemical consumption, potential byproduct formation, and high energy usage, while also failing to address emerging contaminants like perfluoroalkyl acids and pesticides.

Innovation Solution

An advanced oxidation process using oxygen-nanobubbles and UV irradiation generates hydroxyl radicals in-situ, eliminating the need for ozone or hydrogen peroxide, thus reducing chemical and energy costs, and effectively mineralizing recalcitrant contaminants.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional water treatment processes are used, then treatment of microorganisms is achieved, but recalcitrant contaminants such as 1,4-dioxane and PPCPs are not effectively removed

Engineering Contradiction:
Improveremoval effectiveness of recalcitrant contaminantsVSAvoidcapability to address emerging contaminants
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent changes the oxidation mechanism by using UV irradiation to generate hydroxyl radicals from hydrogen peroxide, creating a more powerful oxidizing system that can effectively degrade recalcitrant contaminants like 1,4-dioxane and PPCPs which conventional treatment cannot remove

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent combines multiple treatment mechanisms into a hybrid system that integrates UV irradiation, hydrogen peroxide oxidation, and advanced oxidation processes to create a composite treatment approach capable of addressing both conventional and emerging contaminants

Inventive Principle:
Principle #40Composite materials

2Reliability

If high doses of chlorine are used for disinfection, then microorganism treatment is improved, but disinfection byproducts increase

Engineering Contradiction:
Improvedisinfection effectivenessVSAvoiddisinfection byproducts
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent replaces chemical disinfection (chlorine) with a physical-chemical process using UV irradiation and hydroxyl radicals, which achieves disinfection effectiveness while avoiding the formation of harmful disinfection byproducts associated with chlorine treatment

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Reliability

If advanced oxidation processes are used to remove recalcitrant contaminants, then removal efficiency is improved, but chemical consumption and energy usage increase

Engineering Contradiction:
Improveremoval rate of recalcitrant contaminantsVSAvoidenergy consumption of AOP process
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The patent employs in-situ generation of hydroxyl radicals through UV irradiation of hydrogen peroxide, where the system produces its own oxidizing agents on-demand, reducing the need for external chemical addition and minimizing energy consumption compared to conventional AOP methods

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process achieves rapid and complete removal of recalcitrant contaminants, including 1,4-dioxane and PPCPs, with minimal byproduct formation, achieving removal rates greater than 99.9% in seconds to minutes, and is cost-effective and sustainable.

Implementation Method 1

UV irradiation generates hydroxyl radicals in-situ

Methodology Applied
Scientific EffectPhotodissociation: Photodissociation

Implementation Method 2

oxygen-nanobubble based advanced oxidation process (AOP)... mineralizing recalcitrant contaminants

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentEP4628454A1Removal of dioxane and other recalcitrant contaminants from water using nanobubbles in advanced oxidation processes
Publication Date: 2025.10.08 STREAMGO WATER USA LLC
  • EP4628454A1 patent drawingFigure 1~2
  • EP4628454A1 patent drawingFigure 3~4
  • EP4628454A1 patent drawingFigure 5

AI summary

A method for removing recalcitrant contaminants uses an oxygen-nanobubble advanced oxidation process. Oxygen-nanobubble based advanced oxidation mineralized 1,4 dioxane in an aqueous solution, thereby removing practically all of the 1,4 dioxane. An added advantage is that the process does not form bromate. Also disclosed is an ozone-oxygen nanobubble based advanced oxidation process that removes recalcitrant contaminants. Ozone-oxygen nanobubble based advanced oxidation significantly increased the mass transfer rate compared to that of the micro-bubble technology.