Paraffin-Based Sample Treatment Composition for Single-Step Processing

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Solution Overview

Problem

Current methods for treating biological, cytological, and histological samples require multiple steps and large volumes of solvents, are time-consuming, and often incompatible with automated processors, posing health risks and environmental concerns.

Innovation Solution

A composition comprising paraffin, alcohol, and specific hydrocarbons (naphtha, isoparaffin, or limonene) is used for simultaneous dehydration, clarification, and infiltration in a single step, eliminating ketones and ensuring compatibility with automated processors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If multiple successive steps with ethanol solutions and xylene are used for dehydration and clarification, then the water is effectively removed and compatibility with paraffin is increased, but the processing time increases to about 14 hours and large quantities of solvents (40-45 liters per 1000 samples) are consumed

Engineering Contradiction:
Improvedehydration efficiencyVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The patent combines multiple separate treatment steps (dehydration with ethanol, clarification with xylene, and paraffin infiltration) into a single integrated composition. This composition simultaneously performs all three functions in one bath, reducing processing time from 14 hours to a few hours while eliminating the need for multiple solvent transitions.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The treatment composition is designed to be multi-functional, serving as a universal reagent that performs dehydration, clarification, and paraffin infiltration all at once. This eliminates the need for separate specialized reagents for each step and simplifies the overall processing workflow.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Manufacturing precision

If multiple successive steps with ethanol solutions and xylene are used for dehydration and clarification, then the water is effectively removed and compatibility with paraffin is increased, but the quantity of solvents used increases to 40-45 liters per 1000 samples

Engineering Contradiction:
Improvedehydration efficiencyVSAvoidsolvent consumption
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The patent combines multiple separate treatment steps (dehydration with ethanol, clarification with xylene, and paraffin infiltration) into a single integrated composition. This composition simultaneously performs all three functions in one bath, reducing processing time from 14 hours to a few hours while eliminating the need for multiple solvent transitions.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent eliminates the need to discard and replace multiple different solvents (ethanol, xylene) by using a single reusable composition. The treatment medium serves all purposes throughout the process, eliminating solvent waste and the environmental hazards associated with multiple chemical transitions.

Inventive Principle:
Principle #34Discarding and recovering

3Manufacturing precision

If conventional dehydration and clarification protocols are used, then the sample is properly prepared for paraffin infiltration, but the process is incompatible with automated processors and poses health risks due to solvent exposure

Engineering Contradiction:
Improvesample preparation qualityVSAvoidautomated processor compatibility
Core Design Contradiction:
Manufacturing precisionVSEase of operation

Solution Approach 1:

The treatment composition is designed to be multi-functional, serving as a universal reagent that performs dehydration, clarification, and paraffin infiltration all at once. This eliminates the need for separate specialized reagents for each step and simplifies the overall processing workflow.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent changes the chemical parameters of the treatment medium by using a hydrocarbon-based composition with specific solubility characteristics that enable it to perform multiple functions. The composition's unique chemical properties allow it to dehydrate, clarify, and infiltrate simultaneously, making it compatible with automated processing systems.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution reduces processing time to 1-3 hours, significantly cuts solvent use, and ensures safe handling and environmental sustainability while maintaining sample quality for analysis.

Implementation Method 1

The purpose of these steps is to remove water from the sample to allow its subsequent infiltration in paraffin, which is a hydrophobic substance

Methodology Applied
Scientific EffectHydrophobicity: Hydrophobe

Implementation Method 2

which is able to remove the alcohol and to clearly increase the compatibility with paraffin, in terms of hydrophobicity

Methodology Applied
Scientific EffectHydrophobicity: Hydrophobe

Implementation Method 3

The purpose of the various steps of the dehydration treatment (with ethanol solutions) is to replace the water inside the tissue with solutions of increasing hydrophobicity to make possible the penetration of paraffin, which is a completely hydrophobic substance

Methodology Applied
Scientific EffectHydrophobicity: Hydrophobe

Data Source

PatentEP4232794B1Composition for the treatment of biological, cytological, histological and autopsical samples
Publication Date: 2025.08.06 DIAPATH SPA
  • EP4232794B1 patent drawingFigure 1
  • EP4232794B1 patent drawingFigure 2
  • EP4232794B1 patent drawingFigure 3

AI summary

The present invention relates to a composition for treating biological, cytological, histological and autopsical samples, in particular to a composition capable of merging reagents for the dehydration, clarification and paraffin infiltration treatments of the sample, and to its use in the preparation of samples for analysis.