Parallel Extraction Towers with Diaphragm Pulsation

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Solution Overview

Problem

Conventional liquid-liquid extraction apparatuses face challenges with low liquid-liquid contact efficiency, high installation restrictions due to tall extraction towers, and complex mechanisms, which hinder efficient extraction and maintenance.

Innovation Solution

A multi-tower liquid-liquid extraction apparatus with parallel arranged towers, connected via piping for series liquid channels and diaphragm chambers with adjustable pulsation, utilizing a modified diaphragm pump for efficient pulsation control and reduced height, facilitating easier installation and maintenance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the height of the extraction tower is increased to improve liquid-liquid contact efficiency, then extraction efficiency is improved, but installation restrictions increase and the device becomes more complex

Engineering Contradiction:
Improveextraction efficiencyVSAvoidtower height
Core Design Contradiction:
ProductivityVSLength of stationary object

Solution Approach 1:

The extraction system is divided into multiple separate extraction towers arranged in parallel, each with a reduced height. The towers are connected through piping to form a series liquid channel system, distributing the extraction process across multiple segments rather than requiring a single tall tower.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system transitions from a vertical arrangement (single tall tower) to a horizontal arrangement (multiple parallel towers connected by piping). This dimensional change allows the liquid to flow through multiple towers in series, achieving the required contact efficiency without increasing the height of individual towers.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Productivity

If operating sections are added inside the tower to improve mass transfer, then extraction efficiency is improved, but device complexity and maintenance requirements increase

Engineering Contradiction:
Improvemass transfer efficiencyVSAvoidmechanism complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The diaphragm pump is extracted from the interior of the extraction tower and installed externally. This removes the operating mechanism from the tower, simplifying the internal structure and eliminating maintenance issues associated with internal mechanical components while still achieving pulsation for improved mass transfer.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The diaphragm pump acts as an external intermediary device that provides pulsation to the liquid flow through piping connections. This allows the pump to influence the extraction process without being physically integrated into the tower structure, maintaining simplicity while improving mass transfer efficiency.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If pulsation is applied to the entire column to improve contact efficiency, then liquid-liquid contact efficiency is improved, but flooding occurs and the operating range becomes narrow

Engineering Contradiction:
Improveliquid-liquid contact efficiencyVSAvoidoperating range
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

Pulsation is applied locally at the inlet of each extraction tower rather than uniformly throughout the entire column. The diaphragm pump creates pulsation at the liquid supply point, which then propagates through the packing material. This localized approach improves contact efficiency without causing the flooding that occurs with full-column pulsation.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

Instead of applying pulsation to the entire column volume, the system applies pulsation partially at the inlet region. This partial action is sufficient to generate the desired mixing and contact effects throughout the tower while avoiding the excessive action that leads to flooding and narrow operating ranges.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus enhances liquid contact efficiency and residence time while reducing installation height, offering flexible pulsation control and broader operational range, improving extraction efficiency and ease of maintenance.

Implementation Method 1

a diaphragm pump installed outside the treatment tower is used to provide pulsation to the tower... the internal fluid of the treatment tower is reciprocated

Methodology Applied
Scientific EffectPulsation:

Implementation Method 2

Liquid-liquid extraction process is a process in which desired substances are extracted by transferring solutes dissolved in the solvent to other solvents for separation and purification

Methodology Applied
Scientific EffectLiquid-liquid extraction: Liquid-Liquid Extraction

Implementation Method 3

each extraction tower has a heavy liquid supply portion on the top side of the tower and a heavy liquid discharge portion on the bottom side of the tower, and, has a light liquid supply portion on the bottom side of the tower and a light liquid discharge portion on the top side of the tower

Methodology Applied
Scientific EffectGravity-driven flow: Gravitation

Data Source

PatentUS20240269580A1Liquid-liquid extraction device
Publication Date: 2024.08.15 REFINE HLDG CO LTD
  • US20240269580A1 patent drawing
  • US20240269580A1 patent drawing

AI summary

A multi-tower liquid-liquid extraction apparatus having two or more extraction towers arranged in parallel. Each tower has a heavy-liquid supplying port at the top and a heavy-liquid discharging port at the bottom. Additionally, each tower has a light-liquid supplying port at the bottom and a light-liquid discharging port at the top. The heavy-liquid channels of the extraction towers are connected in series. Furthermore, at least two of the extraction towers are connected to respective diaphragm chambers through their respective piping. These diaphragm chambers have a closed space, part of the wall of which is formed by a diaphragm whose volume is changed by an operating drive section. The piping between each extraction tower and its respective diaphragm chamber is equipped with a pressure-regulating chamber and an on/off valve to regulate the internal pressure.