Parallel Methanation Reactors for SNG Production

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Solution Overview

Problem

Existing SNG production processes require high gas recirculation rates to control exothermal reactions, leading to large and expensive compressors, increased reactor sizes, and higher costs, making the process less competitive with fossil natural gas.

Innovation Solution

Feeding fresh syngas in parallel to multiple reactors with reduced recirculation, where each reactor receives a portion of the fresh syngas and partially converted gas, and using steam addition to control reaction temperatures and equilibrium, thereby reducing the need for extensive gas recirculation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If high gas recirculation rates are used to control exothermal reactions, then reaction temperature is controlled, but compressor size and cost increase significantly

Engineering Contradiction:
Improvereaction temperature controlVSAvoidcompressor power absorption
Core Design Contradiction:
TemperatureVSPower

Solution Approach 1:

The invention divides the single methanation reactor into multiple series-connected reactors (typically 3-5 reactors). Each reactor handles a portion of the conversion, distributing the exothermal heat generation across multiple units. This segmentation allows better temperature control with reduced recirculation ratios, as each reactor operates at lower conversion per pass, reducing the need for excessive dilution with recirculated gas.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention introduces inter-cooling stages between the series-connected reactors as intermediary heat removal mechanisms. Instead of relying solely on gas recirculation for heat control, heat exchangers are placed between reactors to remove excess heat at intermediate stages. This intermediary approach allows temperature control without requiring the same level of gas recirculation, reducing compressor power requirements.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Temperature

If high gas recirculation rates are used to control exothermal reactions, then reaction temperature is controlled, but reactor size and catalyst quantity increase

Engineering Contradiction:
Improvereaction temperature controlVSAvoidreactor volume and catalyst quantity
Core Design Contradiction:
TemperatureVSVolume of stationary object

Solution Approach 1:

By segmenting the methanation process into multiple series reactors, each reactor operates at a lower conversion level per pass. This allows smaller reactor volumes and less catalyst per unit while achieving the same overall conversion. The segmentation distributes the thermal load and allows more efficient use of catalyst bed volume across multiple smaller units rather than one large reactor requiring excessive recirculation.

Inventive Principle:
Principle #1Segmentation

3Temperature

If high gas recirculation rates are used to control exothermal reactions, then reaction temperature is controlled, but production cost increases

Engineering Contradiction:
Improvereaction temperature controlVSAvoidproduction cost
Core Design Contradiction:
TemperatureVSEase of manufacture

Solution Approach 1:

The multi-reactor segmented configuration reduces the overall recirculation ratio required for temperature control, directly reducing compressor power consumption and operational costs. While the number of reactors increases, the reduced catalyst quantity per reactor and lower energy consumption result in overall cost reduction, making SNG production more competitive with fossil natural gas.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The inter-cooling heat exchangers serve as intermediary heat removal devices that reduce the thermal load on the recirculation system. By removing heat at intermediate stages, the system requires less recirculation for temperature control, reducing compressor energy consumption and operational costs while maintaining safe operating temperatures.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Speed

If high gas recirculation rates are used to control exothermal reactions, then reaction rate is controlled, but flow rate through reactors increases

Engineering Contradiction:
Improvereaction rate controlVSAvoidflow rate through reactors
Core Design Contradiction:
SpeedVSProductivity

Solution Approach 1:

By dividing the conversion into multiple series reactors, each reactor operates at a more moderate flow rate with lower conversion per pass. This segmentation allows better control of reaction kinetics without requiring excessive recirculation to dilute the fresh syngas, thus maintaining productivity while controlling the reaction rate through distributed conversion rather than high recirculation dilution.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in a smaller, less expensive compressor and reduced catalyst requirements, lowering operational costs while maintaining effective heat recovery, making SNG production more competitive with fossil fuels.

Implementation Method 1

the above reactions are carried out in a so-called methanation section comprising a plurality of adiabatic reactors with heat recovery and gas recirculation. The reactors contain an appropriate catalyst to increase the yield of the reaction

Methodology Applied
Scientific EffectMethanation reaction: Chemical Bonding

Implementation Method 2

Basically, the process of methanation of the syngas involves the following, strongly exothermal reactions: (I) CO+3 H2 → CH4 + H2O (II) CO2 + 4 H2 → CH4 + 2 H2O where reaction (I) has a thermal output (enthalpy of reaction) of around 206 kJ/mol and reaction (II) of around 165 kJ/mol

Methodology Applied
Scientific EffectExothermal reaction: Exothermic Reaction

Implementation Method 3

heat recovery is provided by heat exchangers cooling the hot gas stream at the outlet of each reactor e.g. by producing high pressure steam

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 4

heat recovery is provided by heat exchangers cooling the hot gas stream at the outlet of each reactor e.g. by producing high pressure steam

Methodology Applied
Scientific EffectPhase change: Phase Change

Implementation Method 5

The gas recirculation requires the provision of an appropriate compressor

Methodology Applied
Scientific EffectGas compression: Gas Compressor

Implementation Method 6

The reactors contain an appropriate catalyst to increase the yield of the reaction

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP2110425B2Process and plant for substitute natural gas
Publication Date: 2022.03.30 CASALE SA
  • EP2110425B2 patent drawingFigure 1

AI summary

A process for producing substitute natural gas (SNG) comprising the steps of reacting a fresh syngas (11) into a methanation section (10) comprising adiabatic reactors (101-104) connected in series, with heat removal and reacted gas-recirculation, wherein the fresh syngas is fed in parallel to said adiabatic reactors. In a preferred embodiment the reacted gas is recirculated to the first reactor (101) and further dilution of the fresh gas at the inlet of the first and second reactor is achieved by steam addition.