Parallel Methanol Separation Unit for Flow Rate Adaptability

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Solution Overview

Problem

The separation of methanol from an outlet stream in methanol synthesis reactors is challenging due to fluctuations in the flow rate caused by renewable energy-powered hydrogen supply, leading to decreased separation performance and risk of liquid droplets passing through separators, potentially damaging downstream compressors.

Innovation Solution

A method utilizing a separation unit with multiple separation devices connected in parallel, where the outlet stream is distributed based on the volume flow rate, allowing the entire stream to pass through one device or be divided among several, ensuring consistent flow velocities and capacities across devices.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If a single separator is used for methanol separation, then the device complexity is low, but the separation efficiency decreases when outlet flow rate fluctuates outside the defined range

Engineering Contradiction:
Improveseparator structureVSAvoidseparation efficiency
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The patent divides a single separator into multiple separation devices connected in parallel. Each separation device can handle a specific portion of the outlet stream, allowing the system to maintain optimal flow velocities across devices even when total outlet flow fluctuates. This segmentation enables the system to adapt to varying flow rates without compromising separation efficiency.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent introduces a flow distribution mechanism that dynamically adjusts the distribution of outlet stream among multiple separation devices based on the total outlet flow rate. This dynamic adjustment ensures that each separation device operates within its optimal flow range, maintaining high separation efficiency across fluctuating operating conditions.

Inventive Principle:
Principle #15Dynamics

2Productivity

If the outlet flow rate increases beyond the defined range, then the productivity increases, but liquid droplets may pass through the separator damaging downstream equipment

Engineering Contradiction:
Improveoutlet flow rateVSAvoidliquid droplet damage
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

By segmenting the separation function across multiple parallel devices, the system can handle higher total outlet flow rates while maintaining safe flow velocities in each individual device. The distributed architecture prevents liquid droplet formation and passage even at elevated productivity levels.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The flow distribution mechanism acts as an intermediary that regulates and distributes the outlet stream among multiple separation devices. This intermediary control ensures that each device receives an appropriate portion of the flow, preventing liquid droplet damage while maintaining high overall productivity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If the outlet flow rate decreases below the defined range, then the productivity decreases, but the separation efficiency also decreases

Engineering Contradiction:
Improveoutlet flow rateVSAvoidseparation efficiency
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The parallel configuration of multiple separation devices allows the system to maintain optimal flow velocities in each device even when total outlet flow is low. By distributing the reduced flow across multiple devices rather than forcing it through a single device, the system maintains separation efficiency while operating at reduced productivity levels.

Inventive Principle:
Principle #1Segmentation

4Adaptability or versatility

If multiple separation devices are used in parallel, then the adaptability to fluctuating flow rates improves, but the device complexity increases

Engineering Contradiction:
Improveflow rate adaptabilityVSAvoidseparation unit structure
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent implements adaptability through segmentation by using multiple identical separation devices in parallel. This modular approach provides flow rate adaptability while keeping individual device complexity low. The standardized parallel configuration simplifies the overall system compared to a single complex adaptive separator.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach ensures reliable methanol separation across varying flow rates, maintaining efficient separation performance and preventing damage to downstream equipment by adjusting the distribution of the outlet stream among multiple separation devices in response to fluctuations in the volume flow rate.

Implementation Method 1

The pre-separator and the main separator are preferably sequentially flowed vertically from bottom to top, so that separated condensate flows downwards by gravity

Methodology Applied
Scientific EffectGravitation: Gravitation

Data Source

PatentEP4474034A1Separation of synthesized methanol
Publication Date: 2024.12.11 LAIR LIQUIDE SA POUR LETUDE & LEXPLOITATION DES PROCEDES GEORGES CLAUDE
  • EP4474034A1 patent drawingFigure 1~2b
  • EP4474034A1 patent drawingFigure 3~4
  • EP4474034A1 patent drawingFigure 5a~5b

AI summary

A process for the synthesis of methanol using a synthesis reactor arrangement (1), wherein methanol produced with the synthesis reactor arrangement (1) is separated from an outlet stream of the synthesis reactor arrangement (1) by a separation unit (2), wherein the separation unit (2) has several separation devices (3.1 to 3.5) connected in parallel in terms of flow technology, wherein the outlet stream is divided among the separation devices (3.1 to 3.5) such that the entire outlet stream is passed through one of the separation devices (3.1 to 3.5) or a portion of the outlet stream is passed through several of the separation devices (3.1 to 3.5), and wherein the distribution of the outlet stream among the separation devices (3.1 to 3.5) is set depending on a volumetric flow rate of the outlet stream.