Parallel Reactor Methanation with Purge Recirculation

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Solution Overview

Problem

Conventional methods for producing methane from CO2-containing gases face challenges in achieving continuous production and maintaining high concentration and purity, often requiring external energy and complex apparatus setups.

Innovation Solution

The use of two or more reactors with CO2 storage-reduction catalysts disposed in parallel, where one reactor stores CO2 and the other reduces it, with a purge gas recirculation system to prevent CO2 emission and enhance methane production using a downstream methanation catalyst.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional methods use a single reactor for CO2 storage and methanation, then the apparatus is simpler, but continuous methane production cannot be achieved

Engineering Contradiction:
Improvecontinuous methane productionVSAvoidapparatus structure
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent divides the single reactor into multiple reactors (first and second reactors) that operate in parallel. Each reactor performs different functions at different times - one stores CO2 while the other produces methane, enabling continuous production without requiring a single complex reactor to handle all functions simultaneously.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent implements periodic switching between CO2 storage mode and methanation mode across the multiple reactors. By alternately switching the functional mode of each reactor in a periodic cycle, the system maintains continuous methane production while keeping each individual reactor relatively simple in design.

Inventive Principle:
Principle #19Periodic action

2Reliability

If purge gas is supplied to remove O2 after CO2 storage, then O2 is effectively removed, but stored CO2 is desorbed and methane concentration decreases

Engineering Contradiction:
ImproveO2 removal efficiencyVSAvoidmethane concentration and purity
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent extracts the O2 removal function from the main methanation process by dedicating specific time periods and reactor configurations solely for purge gas treatment. This separates the oxygen removal step from the methane production step, preventing CO2 desorption during purification and maintaining high methane concentration in the final product.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent performs CO2 storage completely before introducing purge gas for O2 removal. By completing the CO2 uptake phase first and then switching to purge mode, the system ensures maximum CO2 is stored on the catalyst before any desorption can occur, thereby maintaining high methane concentration when methanation begins.

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If CO2 separation and recovery are performed individually before methanation, then CO2 purity is improved, but external energy supply and complex apparatus are required

Engineering Contradiction:
ImproveCO2 purityVSAvoidexternal energy supply
Core Design Contradiction:
Manufacturing precisionVSUse of energy by stationary object

Solution Approach 1:

The patent merges the CO2 separation function and methanation function into a single integrated reactor system using the CO2 storage-reduction catalyst. The catalyst performs both CO2 uptake from the gas mixture and subsequent methanation in the same reactor, eliminating the need for separate CO2 separation apparatus and the external energy they would require.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The CO2 storage-reduction catalyst is designed to perform multiple functions: CO2 adsorption, O2 removal, and methanation. This multi-functional catalyst eliminates the need for separate CO2 separation and purification steps, reducing both apparatus complexity and external energy requirements while maintaining high CO2 purity for methanation.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Productivity

If temperature is raised to 600°C or more for carbon methanation on ferrite, then methane production is achieved, but external energy supply is required

Engineering Contradiction:
Improvemethane production rateVSAvoidexternal energy supply
Core Design Contradiction:
ProductivityVSUse of energy by stationary object

Solution Approach 1:

The patent changes the operating temperature parameter from high temperature (600°C or more) to moderate temperature (250-400°C) by using the CO2 storage-reduction catalyst. This parameter change enables the methanation reaction to proceed at lower temperatures using the heat generated by the reaction itself, eliminating the need for external energy supply while maintaining productive methane generation.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for continuous methane production with improved concentration and purity, preventing CO2 emission and reducing the need for external energy by utilizing heat from the methanation reaction.

Implementation Method 1

a CO2 storage-reduction catalyst having CO2 storage capacity and methane generation ability

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

methane generation ability

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 3

heat generated in the methanation reaction

Methodology Applied
Scientific EffectExothermic Reaction: Exothermic Reaction

Data Source

PatentEP3501632B1Apparatus of producing methane and method for producing methane using the same
Publication Date: 2022.08.10 KK TOYOTA CHUO KENKYUSHO
  • EP3501632B1 patent drawingFigure 1
  • EP3501632B1 patent drawingFigure 2
  • EP3501632B1 patent drawingFigure 3

AI summary

An apparatus of producing methane from a CO2-containing gas comprises: at least two first reactors with a CO2 storage-reduction catalyst having a CO2 storage capacity and a methane generation ability disposed in parallel; at least one second reactor provided with a methanation catalyst; means for supplying purge gas; and means for supplying reducing gas, wherein the means for supplying purge gas and for supplying reducing gas are disposed upstream of the first reactors, the second reactor is disposed downstream of the first reactors, and a gas outlet of one of the first reactors is connected to a gas inlet of at least one different one of the first reactors via a purge gas recirculation line which supplies a purge gas emitted from the gas outlet of the one first reactor into the gas inlet of the different first reactor.